Technology Process of C14H19NO2*ClH
There total 12 articles about C14H19NO2*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
1,4-dioxane;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 2,4,6-trimethyl-pyridine; benzoic acid; (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine / ethanol / 2 h
2: hydrogen / Raney nickel / methanol / 2068.65 Torr
3: N-ethyl-N,N-diisopropylamine / dichloromethane
4: Jones reagent
5: caesium carbonate / N,N-dimethyl-formamide / 20 °C
6: hydrogenchloride / 1,4-dioxane
With
hydrogenchloride; Jones reagent; hydrogen; caesium carbonate; N-ethyl-N,N-diisopropylamine;
(2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; 2,4,6-trimethyl-pyridine; benzoic acid;
In
1,4-dioxane; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
1: Michael Condensation;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogen / Raney nickel / methanol / 2068.65 Torr
2: N-ethyl-N,N-diisopropylamine / dichloromethane
3: Jones reagent
4: caesium carbonate / N,N-dimethyl-formamide / 20 °C
5: hydrogenchloride / 1,4-dioxane
With
hydrogenchloride; Jones reagent; hydrogen; caesium carbonate; N-ethyl-N,N-diisopropylamine;
Raney nickel;
In
1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;