C₆₃H₇₄O₁₃

Base Information

Chemical Name:C₆₃H₇₄O₁₃
CAS No.:1314871-78-7
Molecular Formula:C₆₃H₇₄O₁₃
Molecular Weight:1039.27
Hs Code.:

C<sub>63</sub>H<sub>74</sub>O<sub>13</sub>

Synonyms:C₆₃H₇₄O₁₃

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Chemical Property of C₆₃H₇₄O₁₃

Chemical Property:

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Technology Process of C₆₃H₇₄O₁₃

There total 10 articles about C₆₃H₇₄O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1314871-77-6
C₆₆H₇₈O₁₃

: 1314871-78-7
C₆₃H₇₄O₁₃

Guidance literature:: With acetic acid; In water; at 70 ℃; for 4h;
DOI:10.1016/j.carres.2011.04.032

Reference yield:

: (2R,3R,4R,5S,6R)-1,2,4-tri-O-benzyl-1,2,3,4,5,6-hexahydroxyoct-7-ene

: 1314871-78-7
C₆₃H₇₄O₁₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: pyridinium p-toluenesulfonate / 0.25 h / 20 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -60 °C / Inert atmosphere

2.2: -60 - 20 °C / Inert atmosphere

3.1: n-butyllithium / hexane; toluene / 0 - 20 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: hydrogenchloride / water; acetic acid / 2.5 h / 80 °C

5.1: Hoveyda-Grubbs catalyst second generation / toluene / 1 h / 60 °C / Inert atmosphere

6.1: palladium 10% on activated carbon; hydrogen; triethylamine / ethyl acetate / 2 h / 20 °C / Inert atmosphere

7.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran

8.1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

9.1: acetic acid / water / 4 h / 70 °C

With hydrogenchloride; n-butyllithium; Hoveyda-Grubbs catalyst second generation; oxalyl dichloride; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; pyridinium p-toluenesulfonate; acetic acid; dimethyl sulfoxide; triethylamine; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane; water; acetic acid; ethyl acetate; toluene; 2.1: Swern oxidation / 2.2: Swern oxidation / 3.2: Wittig reaction / 7.1: Mitsunobu reaction;
DOI:10.1016/j.carres.2011.04.032

Reference yield:

: 35958-64-6
3,5,6-Tri-O-benzyl-D-glucofuranose

: 1314871-78-7
C₆₃H₇₄O₁₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

1.2: 0 °C / pH 7 / Inert atmosphere

2.1: pyridinium p-toluenesulfonate / 0.25 h / 20 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -60 °C / Inert atmosphere

3.2: -60 - 20 °C / Inert atmosphere

4.1: n-butyllithium / hexane; toluene / 0 - 20 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

5.1: hydrogenchloride / water; acetic acid / 2.5 h / 80 °C

6.1: Hoveyda-Grubbs catalyst second generation / toluene / 1 h / 60 °C / Inert atmosphere

7.1: palladium 10% on activated carbon; hydrogen; triethylamine / ethyl acetate / 2 h / 20 °C / Inert atmosphere

8.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran

9.1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

10.1: acetic acid / water / 4 h / 70 °C

With hydrogenchloride; n-butyllithium; Hoveyda-Grubbs catalyst second generation; oxalyl dichloride; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; pyridinium p-toluenesulfonate; acetic acid; dimethyl sulfoxide; triethylamine; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane; water; acetic acid; ethyl acetate; toluene; 3.1: Swern oxidation / 3.2: Swern oxidation / 4.2: Wittig reaction / 8.1: Mitsunobu reaction;
DOI:10.1016/j.carres.2011.04.032