3,4,5-TRIACETOXYBENZYL ALCOHOL

Base Information

• Chemical Name: 3,4,5-TRIACETOXYBENZYL ALCOHOL
• CAS No.: 100945-24-2
• Molecular Formula: C13H14 O7
• Molecular Weight: 282.25
• Mol file: 100945-24-2.mol

Synonyms:3,4,5-Triacetoxybenzylalcohol

Chemical Property of 3,4,5-TRIACETOXYBENZYL ALCOHOL

Chemical Property:

• Vapor Pressure: 1.12E-06mmHg at 25°C
• Melting Point: 79-80
• Refractive Index: 1.529
• Boiling Point: 386.8°C at 760 mmHg
• PKA: 13.78±0.10(Predicted)
• Flash Point: 141.5°C
• PSA: 99.13000
• Density: 1.305g/cm³
• LogP: 0.95480

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,4,5-TRIACETOXYBENZYL ALCOHOL

There total 1 articles about 3,4,5-TRIACETOXYBENZYL ALCOHOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

3,4,5-triacetoxybenzoic acid (6635-24-1) → acetic acid 2,3-diacetoxy-5-hydroxymethyl-phenyl ester (100945-24-2)

Guidance literature:

With diborane; In tetrahydrofuran; 1.) 1 h, 0 deg C; 2.) 30 min, room temp.;

Reference yield: 77.0%

acetic acid 2,3-diacetoxy-5-hydroxymethyl-phenyl ester (100945-24-2) → 3,4,5-tri-O-acetylbenzaldehyde (71932-18-8)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; for 1h;

Reference yield:

acetic acid 2,3-diacetoxy-5-hydroxymethyl-phenyl ester (100945-24-2) → 3,4,5-triacetoxybenzyl bromide

Guidance literature:

With carbon tetrabromide; triphenylphosphine; In acetonitrile; at 20 ℃;

upstream raw materials:

3,4,5-triacetoxybenzoic acid

Downstream raw materials:

3,4,5-tri-O-acetylbenzaldehyde

<(S)-N-Acetylleucyl>-<(Z)-3,4,5-triacetoxy-α,β-didehydrophenylalanyl>-<(S)-6-bromtryptophan>

Hexaaxetylcelenamid A

<(S)-N-Acetylleucyl>-<(Z)-3,4,5-triacetoxy-α,β-didehydrophenylalanyl>-<(S)-6-brom-N-<2-(3,4-diacetoxyphenyl)-2-(4-nitrophenylseleno)ethyl>tryptophanamid>