Technology Process of C16H24N2O4*ClH
There total 6 articles about C16H24N2O4*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C16H22N2O6;
With
thiophene; hydrogen;
palladium 10% on activated carbon;
In
ethanol; di-isopropyl ether;
at 20 ℃;
for 20h;
With
hydrogenchloride;
In
1,4-dioxane; ethanol; di-isopropyl ether;
at 0 ℃;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: caesium carbonate / N,N-dimethyl acetamide / 60 °C
2.1: thiophene; hydrogen / palladium 10% on activated carbon / ethanol; di-isopropyl ether / 20 h / 20 °C
2.2: 0 °C
With
thiophene; hydrogen; caesium carbonate;
palladium 10% on activated carbon;
In
ethanol; di-isopropyl ether; N,N-dimethyl acetamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: caesium carbonate / toluene / 0.33 h / 40 °C
1.2: Heating / reflux
2.1: hydrogenchloride / 1,4-dioxane / 30 h / 100 °C
3.1: caesium carbonate / N,N-dimethyl acetamide / 60 °C
4.1: thiophene; hydrogen / palladium 10% on activated carbon / ethanol; di-isopropyl ether / 20 h / 20 °C
4.2: 0 °C
With
thiophene; hydrogenchloride; hydrogen; caesium carbonate;
palladium 10% on activated carbon;
In
1,4-dioxane; ethanol; di-isopropyl ether; N,N-dimethyl acetamide; toluene;