C₃₁H₄₀O₅Si

Base Information

Chemical Name:C₃₁H₄₀O₅Si
CAS No.:1574543-69-3
Molecular Formula:C₃₁H₄₀O₅Si
Molecular Weight:520.741
Hs Code.:

C<sub>31</sub>H<sub>40</sub>O<sub>5</sub>Si

Synonyms:C₃₁H₄₀O₅Si

Suppliers and Price of C₃₁H₄₀O₅Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₁H₄₀O₅Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₁H₄₀O₅Si

There total 6 articles about C₃₁H₄₀O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1574543-50-2
(1S,2S,3aR,6aS)-allyl 2-hydroxy-1-hydroxymethyl-1,2,3,3a,4,6a-hexahydropentalene-1-carboxylate

: 107-30-2
chloromethyl methyl ether

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1574543-69-3
C₃₁H₄₀O₅Si

Guidance literature:: (1S,2S,3aR,6aS)-allyl 2-hydroxy-1-hydroxymethyl-1,2,3,3a,4,6a-hexahydropentalene-1-carboxylate; tert-butylchlorodiphenylsilane; With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 12h; Inert atmosphere;

chloromethyl methyl ether; In dichloromethane; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol5002973

Reference yield:

: 1574543-68-2
C₁₃H₁₆O₄

: 1574543-69-3
C₃₁H₄₀O₅Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tris(acetoxy)borohydride / acetonitrile; acetic acid / 1 h / 0 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

2.2: 12 h / 0 - 20 °C / Inert atmosphere

With dmap; sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetic acid; acetonitrile;
DOI:10.1021/ol5002973

Reference yield:

: (R)-2-oxo-1-phenyl-2-(piperidin-1-yl)ethyl 4-(cyclopent-3-enyl)-2-diazo-3-oxobutanoate

: 1574543-69-3
C₃₁H₄₀O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: dirhodium tetrakis(S-(N-dodecylbenzenesulfonyl)prolinate) / dichloromethane / 8 h / 20 °C / Inert atmosphere

2.1: titanium(IV) isopropylate / 23 h / 60 °C / Inert atmosphere

3.1: formaldehyd; potassium hydrogencarbonate / water / 15 h / -25 °C / Inert atmosphere

4.1: sodium tris(acetoxy)borohydride / acetonitrile; acetic acid / 1 h / 0 °C / Inert atmosphere

5.1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

5.2: 12 h / 0 - 20 °C / Inert atmosphere

With titanium(IV) isopropylate; dmap; formaldehyd; dirhodium tetrakis(S-(N-dodecylbenzenesulfonyl)prolinate); sodium tris(acetoxy)borohydride; potassium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; acetic acid; acetonitrile;
DOI:10.1021/ol5002973