3,6-diphenyl-2-(p-trifluoromethylphenyl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

Base Information

Chemical Name:3,6-diphenyl-2-(p-trifluoromethylphenyl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione
CAS No.:871667-64-0
Molecular Formula:C₂₅H₁₅F₃N₂O₂
Molecular Weight:432.402
Hs Code.:

Synonyms:3,6-diphenyl-2-(p-trifluoromethylphenyl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

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Chemical Property of 3,6-diphenyl-2-(p-trifluoromethylphenyl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

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Technology Process of 3,6-diphenyl-2-(p-trifluoromethylphenyl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

There total 2 articles about 3,6-diphenyl-2-(p-trifluoromethylphenyl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 105194-22-7
2,3-dihydro-2-oxo 5-phenyl-1H-pyrrole-4-carboxylic acid ethyl ester

: N-(p-trifluoromethylphenyl)benzimidoyl chloride

: 871667-64-0
3,6-diphenyl-2-(p-trifluoromethylphenyl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

: ethyl 2-phenyl-4-[1-phenyl-1-(p-trifluoromethylphenylamino)methylidene]-4,5-dihydro-5-oxopyrrole-3-carboxylate

Guidance literature:: 2,3-dihydro-2-oxo-5-phenyl-1H-pyrrole-4-carboxylic acid ethyl ester; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

N-(p-trifluoromethylphenyl)benzimidoyl chloride; In tetrahydrofuran; at 20 ℃; for 168000h;
DOI:10.1016/j.tet.2005.09.005

Reference yield:

: 350-98-1
N-(4-(trifluoromethyl)phenyl)benzamide

: 871667-64-0
3,6-diphenyl-2-(p-trifluoromethylphenyl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride; phosphorus pentachloride / Heating

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C

2.2: 11 percent / tetrahydrofuran / 168000 h / 20 °C

With thionyl chloride; phosphorus pentachloride; sodium hydride; In tetrahydrofuran;
DOI:10.1016/j.tet.2005.09.005