Technology Process of C39H35BClF2N4O6Re
There total 13 articles about C39H35BClF2N4O6Re which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
rhenium(I) pentacarbonyl chloride;
In
toluene;
at 110 ℃;
for 1h;
DOI:10.1039/c2dt32420b
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine; boron trifluoride diethyl etherate / dichloromethane / 12 h / 20 °C
2: N-iodo-succinimide / dichloromethane / 1 h / 10 - 15 °C
3: triethylamine; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; copper(l) iodide / 12 h / Inert atmosphere; Reflux
4: rhenium(I) pentacarbonyl chloride / toluene / 1 h / 110 °C
With
bis-triphenylphosphine-palladium(II) chloride; N-iodo-succinimide; copper(l) iodide; rhenium(I) pentacarbonyl chloride; boron trifluoride diethyl etherate; triethylamine; triphenylphosphine;
In
dichloromethane; toluene;
DOI:10.1039/c2dt32420b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-iodo-succinimide / dichloromethane / 1 h / 10 - 15 °C
2: triethylamine; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; copper(l) iodide / 12 h / Inert atmosphere; Reflux
3: rhenium(I) pentacarbonyl chloride / toluene / 1 h / 110 °C
With
bis-triphenylphosphine-palladium(II) chloride; N-iodo-succinimide; copper(l) iodide; rhenium(I) pentacarbonyl chloride; triethylamine; triphenylphosphine;
In
dichloromethane; toluene;
DOI:10.1039/c2dt32420b
