bis(2-ethylhexyl) (2E)-3-[4-(trifluoromethyl)phenyl]prop-2-en-1-ylphosphate

Base Information

Chemical Name:bis(2-ethylhexyl) (2E)-3-[4-(trifluoromethyl)phenyl]prop-2-en-1-ylphosphate
CAS No.:1542073-99-3
Molecular Formula:C₂₆H₄₂F₃O₄P
Molecular Weight:506.586
Hs Code.:

Synonyms:bis(2-ethylhexyl) (2E)-3-[4-(trifluoromethyl)phenyl]prop-2-en-1-ylphosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(2-ethylhexyl) (2E)-3-[4-(trifluoromethyl)phenyl]prop-2-en-1-ylphosphate

Chemical Property:

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Technology Process of bis(2-ethylhexyl) (2E)-3-[4-(trifluoromethyl)phenyl]prop-2-en-1-ylphosphate

There total 1 articles about bis(2-ethylhexyl) (2E)-3-[4-(trifluoromethyl)phenyl]prop-2-en-1-ylphosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 3658-48-8
bis(2-ethylhexyl)phosphite

: 125617-18-7
3-(4-trifluoromethylphenyl)-2-propen-1-ol

: 1542073-99-3
bis(2-ethylhexyl) (2E)-3-[4-(trifluoromethyl)phenyl]prop-2-en-1-ylphosphate

Guidance literature:: With tetrabutylammomium bromide; sodium hydroxide; In tetrachloromethane; dichloromethane; water; at 0 ℃; for 3.5h; Inert atmosphere;
DOI:10.1021/ja411869r

Reference yield:

: 1542073-99-3
bis(2-ethylhexyl) (2E)-3-[4-(trifluoromethyl)phenyl]prop-2-en-1-ylphosphate

: 77485-20-2
trans-potassium crotonate

: 1542074-88-3
(+)-(1R)-1-[4-(trifluoromethyl)phenyl]prop-2-en-1-yl (2E)-but-2-enoate

: C₁₄H₁₃F₃O₂

Guidance literature:: With C₅₈H₅₂IrNO₄P⁽¹⁺⁾; In tert-butyl methyl ether; at 20 ℃; for 7.5h; Overall yield = 60 %; Overall yield = 65.3 mg; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja411869r

Reference yield:

: 1542073-99-3
bis(2-ethylhexyl) (2E)-3-[4-(trifluoromethyl)phenyl]prop-2-en-1-ylphosphate

: 77485-20-2
trans-potassium crotonate

: C₁₄H₁₃F₃O₂

: 1373125-97-3
C₁₄H₁₃F₃O₂

Guidance literature:: With C₅₈H₅₂IrNO₄P⁽¹⁺⁾; In tetrahydrofuran; at 20 ℃; for 0.75h; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja411869r