C₂₂H₂₂F₃NO₆S

Base Information

Chemical Name:C₂₂H₂₂F₃NO₆S
CAS No.:1379449-95-2
Molecular Formula:C₂₂H₂₂F₃NO₆S
Molecular Weight:485.481
Hs Code.:

C<sub>22</sub>H<sub>22</sub>F<sub>3</sub>NO<sub>6</sub>S

Synonyms:C₂₂H₂₂F₃NO₆S

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Chemical Property of C₂₂H₂₂F₃NO₆S

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Technology Process of C₂₂H₂₂F₃NO₆S

There total 7 articles about C₂₂H₂₂F₃NO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1379449-79-2
C₂₇H₃₀F₃NO₈S

: 1379449-95-2
C₂₂H₂₂F₃NO₆S

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/ja301326k

Reference yield:

: 1379449-94-1
C₂₁H₃₂N₂O₆

: 1379449-95-2
C₂₂H₂₂F₃NO₆S

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / -78 - 0 °C / Inert atmosphere

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 25 °C

3: tetrahydrofuran / 0 - 25 °C / Inert atmosphere; Molecular sieve

4: pyridinium chlorochromate / dichloromethane / 4 h / 25 °C / Inert atmosphere; Molecular sieve

5: 2,6-di-tert-butyl-pyridine / nitromethane / 2 h / -20 °C / Inert atmosphere; Molecular sieve

6: trifluorormethanesulfonic acid / dichloromethane / 1 h / 0 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,6-di-tert-butyl-pyridine; trifluorormethanesulfonic acid; pyridinium chlorochromate; In tetrahydrofuran; nitromethane; dichloromethane; 5: Friedel Crafts acylation;
DOI:10.1021/ja301326k

Reference yield:

: 1379449-82-7
C₂₁H₂₉NO₅

: 1379449-95-2
C₂₂H₂₂F₃NO₆S

Guidance literature:: Multi-step reaction with 5 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 25 °C

2: tetrahydrofuran / 0 - 25 °C / Inert atmosphere; Molecular sieve

3: pyridinium chlorochromate / dichloromethane / 4 h / 25 °C / Inert atmosphere; Molecular sieve

4: 2,6-di-tert-butyl-pyridine / nitromethane / 2 h / -20 °C / Inert atmosphere; Molecular sieve

5: trifluorormethanesulfonic acid / dichloromethane / 1 h / 0 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,6-di-tert-butyl-pyridine; trifluorormethanesulfonic acid; pyridinium chlorochromate; In tetrahydrofuran; nitromethane; dichloromethane; 4: Friedel Crafts acylation;
DOI:10.1021/ja301326k