(3S,8S,9S,10R,11S,13S,14S,17S)-10,13,17-trimethyl-1,2,3,4,7,8,9,11,12, 14,15,16-dodecahydrocyclopenta[a]phenanthrene-3,11,17-triol

Base Information

• Chemical Name: (3S,8S,9S,10R,11S,13S,14S,17S)-10,13,17-trimethyl-1,2,3,4,7,8,9,11,12, 14,15,16-dodecahydrocyclopenta[a]phenanthrene-3,11,17-triol
• CAS No.: 5446-39-9
• Molecular Formula: C₂₀H₃₂O₃
• Molecular Weight: 320.472
• Mol file: 5446-39-9.mol

Synonyms:NSC17252;(3S,8S,9S,10R,11S,13S,14S,17S)-10,13,17-Trimethyl-1,2,3,4,7,8,9,11,12, 14,15,16-dodecahydrocyclopenta[a]phenanthrene-3,11,17-triol;17-Methylandrost-5-ene-3β,11β,17β-triol;(3β,11β,17β)-17-Methylandrost-5-ene-3,11,17-triol;

Chemical Property of (3S,8S,9S,10R,11S,13S,14S,17S)-10,13,17-trimethyl-1,2,3,4,7,8,9,11,12, 14,15,16-dodecahydrocyclopenta[a]phenanthrene-3,11,17-triol

Chemical Property:

• Vapor Pressure: 7.72E-11mmHg at 25°C
• Refractive Index: 1.581
• Boiling Point: 470.7 °C at 760 mmHg
• Flash Point: 213 °C
• PSA: 60.69000
• Density: 1.17 g/cm³
• LogP: 3.03190

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3S,8S,9S,10R,11S,13S,14S,17S)-10,13,17-trimethyl-1,2,3,4,7,8,9,11,12, 14,15,16-dodecahydrocyclopenta[a]phenanthrene-3,11,17-triol

There total 3 articles about (3S,8S,9S,10R,11S,13S,14S,17S)-10,13,17-trimethyl-1,2,3,4,7,8,9,11,12, 14,15,16-dodecahydrocyclopenta[a]phenanthrene-3,11,17-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

11β-hydroxy-17α-methyltestosterone (1043-10-3) → 17-methyl-androst-5-ene-3β,11β,17β-triol (5446-39-9)

Guidance literature:

ueber mehrere Stufen;

Reference yield:

→ 17α-Methyl-androst-5-en-3β,11β,17β-triol (5446-39-9)

Guidance literature:

aus 11β-Hydroxy-17α-methyltestosteron und LiAlH4;

Reference yield:

→ 17α-Methyl-5-androsten-3β,11β,17β-triol (5446-39-9)

Guidance literature:

11β-Hydroxy-17α-methyltestosteron, 1)Ac2O-p-TsOH 2)NaBH4 3)LiAlH4;

upstream raw materials:

11β-hydroxy-17α-methyltestosterone

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