8-chloro-7,7-bis(dimethylphenylphosphine)-nido-7-platinaundecaborane

Base Information

Chemical Name:8-chloro-7,7-bis(dimethylphenylphosphine)-nido-7-platinaundecaborane
CAS No.:96029-10-6
Molecular Formula:C₁₆H₃₃B₁₀ClP₂Pt
Molecular Weight:626.029
Hs Code.:

Synonyms:8-chloro-7,7-bis(dimethylphenylphosphine)-nido-7-platinaundecaborane

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Chemical Property of 8-chloro-7,7-bis(dimethylphenylphosphine)-nido-7-platinaundecaborane

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Technology Process of 8-chloro-7,7-bis(dimethylphenylphosphine)-nido-7-platinaundecaborane

There total 2 articles about 8-chloro-7,7-bis(dimethylphenylphosphine)-nido-7-platinaundecaborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 15393-14-3,38928-82-4,30759-88-7
[PtCl₂(PMe₂Ph)2]

: 28377-92-6
bis(dimethyl sulfide) arachno-decaborane⁽¹⁴⁾

: 75309-24-9
[7,7-(PMe₂Ph)2-nido-7-PtB₁₀H₁₂]

: S(CH₃)2B₉H₁₃

: 96029-10-6
8-chloro-7,7-bis(dimethylphenylphosphine)-nido-7-platinaundecaborane

Guidance literature:: In dichloromethane; The mixt. of reagents in CH2Cl2 was heated under reflux for 4 h or stirred for 36 h at room temp. (N2 atm.);; evapd., chromd. by preparative TLC; elem. anal.;;

Reference yield: 15.0%

: 15393-14-3,38928-82-4,30759-88-7
[PtCl₂(PMe₂Ph)2]

: 28377-92-6
bis(dimethyl sulfide) arachno-decaborane⁽¹⁴⁾

: 17702-41-9
nido-decaborane

: 2P(CH₃)2C₆H₅*Pt₂B₁₂H₁₈=(P(CH₃)2C₆H₅)2(Pt₂B₁₂H₁₈)

: 75309-24-9
[7,7-(PMe₂Ph)2-nido-7-PtB₁₀H₁₂]

: S(CH₃)2B₉H₁₃

: 96029-10-6
8-chloro-7,7-bis(dimethylphenylphosphine)-nido-7-platinaundecaborane

Guidance literature:: In diethyl ether; dichloromethane; The mixt. of reagents in CH2Cl2-Et2O was heated under reflux for 4 h orstirred for 36 h at room temp. (N2 atm.);; evapd., chromd. by preparative TLC; elem. anal.;;