methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2-O-acetyl-3-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside

Base Information

Chemical Name:methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2-O-acetyl-3-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside
CAS No.:1261355-73-0
Molecular Formula:C₄₉H₆₆O₂₀S
Molecular Weight:1007.12
Hs Code.:

methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2-O-acetyl-3-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside

Synonyms:methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2-O-acetyl-3-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside

Suppliers and Price of methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2-O-acetyl-3-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2-O-acetyl-3-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2-O-acetyl-3-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside

There total 4 articles about methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2-O-acetyl-3-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1161813-90-6
C₂₃H₃₀O₈S

: 1261355-56-9
methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-2-O-acetyl-3-O-methyl-1-O-trichloroacetimidoyl-D-glucopyranosyluronate

: 1261355-73-0
methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2-O-acetyl-3-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside

: methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2-O-acetyl-3-O-methyl-α-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 - 20 ℃; for 12h; Molecular sieve;
DOI:10.1016/j.tetlet.2010.10.042

Reference yield:

: methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2-O-acetyl-3-O-methyl-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside

: 1261355-73-0
methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2-O-acetyl-3-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol;
DOI:10.1016/j.tet.2012.06.081

Reference yield:

: methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-2-O-acetyl-3-O-methyl-D-glucopyranosyluronate

: 1261355-73-0
methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2-O-acetyl-3-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.5 h / 0 °C

2: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h / -20 - 0 °C / Molecular sieve; Inert atmosphere

3: sodium methylate / methanol

With trimethylsilyl trifluoromethanesulfonate; sodium methylate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; dichloromethane;
DOI:10.1016/j.tet.2012.06.081