3-(N-(2-cyclohexylamino-2-oxoethyl)-N-sulfamoyl)benzamidine

Base Information

Chemical Name:3-(N-(2-cyclohexylamino-2-oxoethyl)-N-sulfamoyl)benzamidine
CAS No.:1403957-50-5
Molecular Formula:C₁₅H₂₂N₄O₃S
Molecular Weight:338.431
Hs Code.:

Synonyms:3-(N-(2-cyclohexylamino-2-oxoethyl)-N-sulfamoyl)benzamidine

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Chemical Property of 3-(N-(2-cyclohexylamino-2-oxoethyl)-N-sulfamoyl)benzamidine

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Technology Process of 3-(N-(2-cyclohexylamino-2-oxoethyl)-N-sulfamoyl)benzamidine

There total 5 articles about 3-(N-(2-cyclohexylamino-2-oxoethyl)-N-sulfamoyl)benzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₄N₄O₅S

: 1403957-50-5
3-(N-(2-cyclohexylamino-2-oxoethyl)-N-sulfamoyl)benzamidine

Guidance literature:: With 10% Pd/C; hydrogen; In acetic acid; at 20 ℃; for 1h; under 2280.15 Torr;
DOI:10.1016/j.bmc.2012.08.042

Reference yield:

: 3496-41-1
cyclohexyl carbamoylmethyl carbamic acid benzyl ester

: 1403957-50-5
3-(N-(2-cyclohexylamino-2-oxoethyl)-N-sulfamoyl)benzamidine

Guidance literature:: Multi-step reaction with 5 steps

1: 10% Pd/C; hydrogen / ethyl acetate / 2280.15 Torr

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 20 °C

3: hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / ethanol / 1 h / 87 °C

4: acetonitrile / 1 h / 20 °C

5: 10% Pd/C; hydrogen / acetic acid / 1 h / 20 °C / 2280.15 Torr

With 10% Pd/C; hydroxylamine hydrochloride; hydrogen; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; acetic acid; ethyl acetate; acetonitrile;
DOI:10.1016/j.bmc.2012.08.042

Reference yield:

: 1372089-88-7
2-(3-cyanophenylsulfonamido)-N-cyclohexylacetamide

: 1403957-50-5
3-(N-(2-cyclohexylamino-2-oxoethyl)-N-sulfamoyl)benzamidine

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / ethanol / 1 h / 87 °C

2: acetonitrile / 1 h / 20 °C

3: 10% Pd/C; hydrogen / acetic acid / 1 h / 20 °C / 2280.15 Torr

With 10% Pd/C; hydroxylamine hydrochloride; hydrogen; N-ethyl-N,N-diisopropylamine; In ethanol; acetic acid; acetonitrile;
DOI:10.1016/j.bmc.2012.08.042