3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaure

Base Information

• Chemical Name: 3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaure
• CAS No.: 116527-91-4
• Molecular Formula: C₂₃H₂₄N₂O₄
• Molecular Weight: 392.455

Synonyms:3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaure

Chemical Property of 3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaure

Chemical Property:

Purity/Quality:

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Technology Process of 3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaure

There total 2 articles about 3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurenitril (114476-24-3) → 3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaure (116527-91-4)

Guidance literature:

With methanol; sodium hydroxide; for 16h; Heating;

DOI:10.1016/S0040-4020(01)86862-9

Reference yield: 79.0%

3-benzyloxy-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester (114476-15-2) → 3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaure (116527-91-4)

Guidance literature:

With sodium hydroxide; water; In ethanol; for 0.75h;

DOI:10.1016/S0040-4020(01)86862-9

Reference yield: 96.0%

2,3,4,5,6-pentafluorophenol (771-61-9) + 3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaure (116527-91-4) → 3-benzyloxycarbonyl-7-pentafluorphenyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol (116527-92-5)

Guidance literature:

With dicyclohexyl-carbodiimide; In ethyl acetate; for 2h; Ambient temperature;

DOI:10.1016/S0040-4020(01)86862-9

upstream raw materials:

3-benzyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsaurenitril

3-benzyloxy-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

Downstream raw materials:

3-benzyloxy-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

3-benzyloxycarbonyl-7-pentafluorphenyloxycarbonyl-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol

4b-Chloro-5,6,8,9,10,11-hexahydro-4bH-7,12-diaza-cyclonona[a]indene-7,11-dicarboxylic acid 7-benzyl ester 11-methyl ester

3-benzyloxycarbonyl-7-methoxy-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

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