N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-3-fluorobenzamide

Base Information

Chemical Name:N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-3-fluorobenzamide
CAS No.:2824-15-9
Molecular Formula:C₁₈H₁₆FN₃O₂
Molecular Weight:325.342
Hs Code.:
Mol file:2824-15-9.mol

Synonyms:N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-3-fluorobenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-3-fluorobenzamide

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Technology Process of N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-3-fluorobenzamide

There total 2 articles about N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-3-fluorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 83-07-8
4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one

: 1711-07-5
3-fluorobenzoyl chloride

: 2824-15-9
N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-3-fluorobenzamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/ejoc.202100513

Reference yield:

: 2824-15-9
N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-3-fluorobenzamide

Guidance literature:: aus 4-Aminoantipyrin und 3-Fluorbenzoesaeure in Gegenwart von PCl3 in Bzl.bei 3 Std.Δ auf 100grad(Bzl.);

Reference yield: 95.0%

: 106-38-7
para-bromotoluene

: 2824-15-9
N-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-3-fluorobenzamide

: 4-fluoro-4'-methylbiphenyl-2-carboxylic acid (1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)amide

Guidance literature:: With tris(triphenylphosphine)ruthenium(II) chloride; sodium carbonate; In toluene; at 140 ℃; for 24h;
DOI:10.1002/ejoc.202100513