3,8,13,18-Tetrakis(2,4,6-tri-tert-butylphenyl)-3,8,13,18-tetraphosphaicosa-1,4,6,9,11,14,16,19-octayne

Base Information

Chemical Name:3,8,13,18-Tetrakis(2,4,6-tri-tert-butylphenyl)-3,8,13,18-tetraphosphaicosa-1,4,6,9,11,14,16,19-octayne
CAS No.:313703-91-2
Molecular Formula:C₈₈H₁₁₈P₄
Molecular Weight:1299.8
Hs Code.:

Synonyms:3,8,13,18-Tetrakis(2,4,6-tri-tert-butylphenyl)-3,8,13,18-tetraphosphaicosa-1,4,6,9,11,14,16,19-octayne

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Chemical Property of 3,8,13,18-Tetrakis(2,4,6-tri-tert-butylphenyl)-3,8,13,18-tetraphosphaicosa-1,4,6,9,11,14,16,19-octayne

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Technology Process of 3,8,13,18-Tetrakis(2,4,6-tri-tert-butylphenyl)-3,8,13,18-tetraphosphaicosa-1,4,6,9,11,14,16,19-octayne

There total 2 articles about 3,8,13,18-Tetrakis(2,4,6-tri-tert-butylphenyl)-3,8,13,18-tetraphosphaicosa-1,4,6,9,11,14,16,19-octayne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 313703-89-8
3,8,13,18-Tetrakis(2,4,6-tri-tert-butylphenyl)-1,20-bis(triisopropylsilyl)-3,8,13,18-tetraphosphaicosa-1,4,6,9,11,14,16,19-octayne

: 313703-91-2
3,8,13,18-Tetrakis(2,4,6-tri-tert-butylphenyl)-3,8,13,18-tetraphosphaicosa-1,4,6,9,11,14,16,19-octayne

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -78 ℃; for 2h;
DOI:10.1002/1521-3765(20001016)6:20<3806::AID-CHEM3806>3.0.CO;2-J

Reference yield: 33.0%

: 313703-89-8
3,8,13,18-Tetrakis(2,4,6-tri-tert-butylphenyl)-1,20-bis(triisopropylsilyl)-3,8,13,18-tetraphosphaicosa-1,4,6,9,11,14,16,19-octayne

: 313703-91-2
3,8,13,18-Tetrakis(2,4,6-tri-tert-butylphenyl)-3,8,13,18-tetraphosphaicosa-1,4,6,9,11,14,16,19-octayne

: 3,8,13,18-Tetrakis(2,4,6-tri-tert-butylphenyl)-1-(triisopropylsilyl)-3,8,13,18-tetraphosphaicosa-1,4,6,9,11,14,16,19-octayne

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -78 ℃; for 2h;
DOI:10.1002/1521-3765(20001016)6:20<3806::AID-CHEM3806>3.0.CO;2-J

Reference yield: 65.0%

: 313703-91-2
3,8,13,18-Tetrakis(2,4,6-tri-tert-butylphenyl)-3,8,13,18-tetraphosphaicosa-1,4,6,9,11,14,16,19-octayne

: 1,6,11,16-tetrakis-(2,4,6-tri-tert-butyl-phenyl)-1,6,11,16tetraphospha-cycloeicosa-2,4,7,9,12,14,17,19-octayne

: C₁₇₆H₂₃₂P₈

Guidance literature:: With pyridine; copper diacetate; copper(l) chloride; In methanol; at 20 ℃; for 10h; Title compound not separated from byproducts;
DOI:10.1002/1521-3765(20001016)6:20<3806::AID-CHEM3806>3.0.CO;2-J