1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene

Base Information

Chemical Name:1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene
CAS No.:102393-16-8
Molecular Formula:C₃₈H₅₆N₂O₄
Molecular Weight:604.874
Hs Code.:

Synonyms:1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene

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Chemical Property of 1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene

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Technology Process of 1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene

There total 15 articles about 1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.3%

: 102410-88-8
1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)-5-oxopentyl>-2,3,5,6-tetramethylbenzene

: 102393-16-8
1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene

Guidance literature:: With diborane; In tetrahydrofuran;

Reference yield:

: 3022-16-0
1,4-bis(chloromethyl)-2,3,5,6-tetramethylbenzene

: 102393-16-8
1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene

Guidance literature:: Multi-step reaction with 12 steps

1: 1.) Na / 1.) ethanol; 2.) ethanol, reflux, 0.5 h

2: H₂O, KOH / Heating

3: 94.7 percent / quinoline / 0.33 h / Heating

4: 89.4 percent / cc. H₂SO₄ / toluene

5: 89.6 percent / B₂H₆ / tetrahydrofuran

6: 91.2 percent / 48 percent HBr / H₂O / 0.5 h / Heating

7: 1.) Na / 1.) ethanol; 2.) ethanol, reflux

8: H₂O, KOH / Heating

9: 94.6 percent / quinoline / 0.33 h / Heating

10: SOCl₂ / Heating

11: SnCl₂ / CH₂Cl₂; nitromethane / 1 h / Ambient temperature

12: 88.3 percent / B₂H₆ / tetrahydrofuran

With quinoline; potassium hydroxide; thionyl chloride; sulfuric acid; water; hydrogen bromide; sodium; tin(ll) chloride; diborane; In tetrahydrofuran; nitromethane; dichloromethane; water; toluene;

Reference yield:

: 102393-11-3
5-[4-(4-Chlorocarbonyl-butyl)-2,3,5,6-tetramethyl-phenyl]-pentanoyl chloride

: 102393-16-8
1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: SnCl₂ / CH₂Cl₂; nitromethane / 1 h / Ambient temperature

2: 88.3 percent / B₂H₆ / tetrahydrofuran

With tin(ll) chloride; diborane; In tetrahydrofuran; nitromethane; dichloromethane;