5-Methylcarbonylpentyl-2-deoxy beta-D-Glucopyranoside

Base Information

• Chemical Name: 5-Methylcarbonylpentyl-2-deoxy beta-D-Glucopyranoside
• CAS No.: 100605-25-2
• Molecular Formula: C15H27 N O8
• Molecular Weight: 276.32606
• Mol file: 100605-25-2.mol

Synonyms:5-Methylcarbonylpentyl-2-deoxy beta-D-Glucopyranoside

Chemical Property of 5-Methylcarbonylpentyl-2-deoxy beta-D-Glucopyranoside

Chemical Property:

• PSA: 96.22000
• LogP: -0.01850

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Methylcarbonylpentyl-2-deoxy beta-D-Glucopyranoside

There total 3 articles about 5-Methylcarbonylpentyl-2-deoxy beta-D-Glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(methoxycarbonyl)pentyl 2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-galactopyranoside (100605-24-1) → 5-(methoxycarbonyl)pentyl 2-acetamido-2-deoxy-β-D-galactopyranoside (100605-25-2)

Guidance literature:

With sodium methylate; In methanol;

DOI:10.1021/ja00268a056

Reference yield:

hexahydro-2H-oxepin-2-one (502-44-3,24980-41-4,80137-66-2) → 5-(methoxycarbonyl)pentyl 2-acetamido-2-deoxy-β-D-galactopyranoside (100605-25-2)

Guidance literature:

Multi-step reaction with 3 steps

1: NaOMe / 5 h / Ambient temperature

3: 0.5M NaOMe / methanol

With sodium methylate; In methanol;

DOI:10.1021/ja00268a056

Reference yield:

methyl 6-hydroxycaproate (4547-43-7) → 5-(methoxycarbonyl)pentyl 2-acetamido-2-deoxy-β-D-galactopyranoside (100605-25-2)

Guidance literature:

Multi-step reaction with 2 steps

2: 0.5M NaOMe / methanol

With sodium methylate; In methanol;

DOI:10.1021/ja00268a056

upstream raw materials:

5-(methoxycarbonyl)pentyl 2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-galactopyranoside

hexahydro-2H-oxepin-2-one

methyl 6-hydroxycaproate

Downstream raw materials:

5-(methoxycarbonyl)pentyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-galactopyranoside

6-((4aR,6R,7R,8R,8aR)-7-Acetylamino-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-hexanoic acid methyl ester