C₁₄H₁₀F₃N₅

Base Information

Chemical Name:C₁₄H₁₀F₃N₅
CAS No.:1228788-30-4
Molecular Formula:C₁₄H₁₀F₃N₅
Molecular Weight:305.262
Hs Code.:

C<sub>14</sub>H<sub>10</sub>F<sub>3</sub>N<sub>5</sub>

Synonyms:C₁₄H₁₀F₃N₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₀F₃N₅

Chemical Property:

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Technology Process of C₁₄H₁₀F₃N₅

There total 6 articles about C₁₄H₁₀F₃N₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1228788-29-1
C₁₄H₇F₃N₄

: 1228788-30-4
C₁₄H₁₀F₃N₅

Guidance literature:: With trimethylaluminum; ammonium chloride; In toluene; at 110 ℃; for 3h;

Reference yield:

: 106861-14-7
2-[(4-methylphenyl)sulfonyl]-2,3-dihydropyridazine-3-carbonitrile

: 1228788-30-4
C₁₄H₁₀F₃N₅

Guidance literature:: Multi-step reaction with 7 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.5 h / 20 °C

2: hydrogenchloride; hydrogen / palladium on activated charcoal / water; methanol / 2 h / 2068.65 Torr

3: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 20 °C

4: trichlorophosphate / 1,2-dichloro-ethane / 3 h / Reflux

5: N-iodo-succinimide / acetonitrile / 0.33 h / Reflux

6: 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / N,N-dimethyl-formamide; water / 1 h / 110 °C

7: ammonium chloride; trimethylaluminum / toluene / 3 h / 110 °C

With hydrogenchloride; N-iodo-succinimide; hydrogen; trimethylaluminum; ammonium chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trichlorophosphate; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 1228788-26-8
C₁₃H₁₀F₃N₃O

: 1228788-30-4
C₁₄H₁₀F₃N₅

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / 1,2-dichloro-ethane / 3 h / Reflux

2: N-iodo-succinimide / acetonitrile / 0.33 h / Reflux

3: 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / N,N-dimethyl-formamide; water / 1 h / 110 °C

4: ammonium chloride; trimethylaluminum / toluene / 3 h / 110 °C

With N-iodo-succinimide; trimethylaluminum; ammonium chloride; trichlorophosphate; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; acetonitrile;