C₁₄H₂₀O₅S

Base Information

Chemical Name:C₁₄H₂₀O₅S
CAS No.:40093-80-9
Molecular Formula:C₁₄H₂₀O₅S
Molecular Weight:300.376
Hs Code.:

C<sub>14</sub>H<sub>20</sub>O<sub>5</sub>S

Synonyms:C₁₄H₂₀O₅S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₂₀O₅S

Chemical Property:

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Technology Process of C₁₄H₂₀O₅S

There total 1 articles about C₁₄H₂₀O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: C₂₁H₂₄O₅S

: 40093-80-9
C₁₄H₂₀O₅S

Guidance literature:: With acetyl chloride; In methanol; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.201300935

Reference yield: 86.0%

: 40093-80-9
C₁₄H₂₀O₅S

: 98-59-9
p-toluenesulfonyl chloride

: 1585246-32-7
C₂₁H₂₆O₇S₂

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 16h; Inert atmosphere;
DOI:10.1002/ejoc.201300935

Reference yield:

: 40093-80-9
C₁₄H₂₀O₅S

: 1585246-51-0
C₁₇H₁₈N₂O₅S

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / dichloromethane / 16 h / 0 °C / Inert atmosphere

2: dmap; pyridine / 24 h / 0 - 20 °C / Inert atmosphere

3: sodium hydroxide / 1,4-dioxane / 1 h / Inert atmosphere; Reflux

4: magnesium bis(monoperoxyphthalate)hexahydrate / methanol / 6 h / 20 °C / Inert atmosphere

5: pyridine; methanesulfonyl chloride / 16 h / 0 - 4 °C / Inert atmosphere

6: potassium tert-butylate / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

With pyridine; dmap; magnesium bis(monoperoxyphthalate)hexahydrate; potassium tert-butylate; methanesulfonyl chloride; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;
DOI:10.1002/ejoc.201300935