ethyl 4-(2,3-dihydro-8-methoxy-1,4-benzodioxin-5-yl)-3-cyclohexenecarboxylate

Base Information

Chemical Name:ethyl 4-(2,3-dihydro-8-methoxy-1,4-benzodioxin-5-yl)-3-cyclohexenecarboxylate
CAS No.:444108-39-8
Molecular Formula:C₁₈H₂₂O₅
Molecular Weight:318.37
Hs Code.:

Synonyms:ethyl 4-(2,3-dihydro-8-methoxy-1,4-benzodioxin-5-yl)-3-cyclohexenecarboxylate

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Chemical Property of ethyl 4-(2,3-dihydro-8-methoxy-1,4-benzodioxin-5-yl)-3-cyclohexenecarboxylate

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Technology Process of ethyl 4-(2,3-dihydro-8-methoxy-1,4-benzodioxin-5-yl)-3-cyclohexenecarboxylate

There total 10 articles about ethyl 4-(2,3-dihydro-8-methoxy-1,4-benzodioxin-5-yl)-3-cyclohexenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.4%

: 444108-43-4
4-(2,3-dihydro-8-methoxy-1,4-benzodioxin-5-yl)-3-cyclohexenecarboxylic acid

: 444108-39-8
ethyl 4-(2,3-dihydro-8-methoxy-1,4-benzodioxin-5-yl)-3-cyclohexenecarboxylate

Guidance literature:: With ethanol; sulfuric acid; In water; for 3h; Product distribution / selectivity; Heating / reflux;

Reference yield: 82.0%

: 444108-40-1
8-methoxy-2,3-dihydrobenzo[b][1,4]dioxin-5-ylboronic acid

: 122948-57-6
ethyl 4-(((trifluoromethyl)sulfonyl)oxy)cyclohex-3-enecarboxylate

: 444108-39-8
ethyl 4-(2,3-dihydro-8-methoxy-1,4-benzodioxin-5-yl)-3-cyclohexenecarboxylate

Guidance literature:: With 10% palladium on carbon; potassium carbonate; triphenylphosphine; In 1,2-dimethoxyethane; water; ethyl acetate; for 3h; Inert atmosphere; Reflux;
DOI:10.1021/ol902244e

Reference yield: 73.2%

: ethyl 4-trifluoromethanesulfonyl-3-cyclohexenecarboxylate

: (2,3-dihydro-8-methoxy-1,4-benzodioxine-5-yl)boric acid

: 444108-39-8
ethyl 4-(2,3-dihydro-8-methoxy-1,4-benzodioxin-5-yl)-3-cyclohexenecarboxylate

Guidance literature:: With sodium carbonate; triphenylphosphine; lithium bromide; 5%-palladium/activated carbon; In 1,2-dimethoxyethane; water; for 1h; Product distribution / selectivity; Heating / reflux;