Technology Process of C17H21N
There total 4 articles about C17H21N which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 0 ℃;
Reflux;
DOI:10.1021/jacs.5b10267
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.42 h / 0 - 20 °C
1.2: 80 °C / Cooling with ice
2.1: palladium on activated charcoal; hydrogen / ethyl acetate; methanol / 12 h / 20 °C / Inert atmosphere
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux
With
lithium aluminium tetrahydride; palladium on activated charcoal; hydrogen; sodium hydride;
In
tetrahydrofuran; methanol; ethyl acetate; mineral oil;
DOI:10.1021/jacs.5b10267
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium on activated charcoal; hydrogen / ethyl acetate; methanol / 12 h / 20 °C / Inert atmosphere
2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux
With
lithium aluminium tetrahydride; palladium on activated charcoal; hydrogen;
In
tetrahydrofuran; methanol; ethyl acetate;
DOI:10.1021/jacs.5b10267