phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4-tri-O-methyl-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4-tri-O-methyl-1-thio-α-D-mannopyranoside
CAS No.:1391727-78-8
Molecular Formula:C₄₉H₄₈O₁₄S
Molecular Weight:892.978
Hs Code.:

Synonyms:phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4-tri-O-methyl-1-thio-α-D-mannopyranoside

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Chemical Property of phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4-tri-O-methyl-1-thio-α-D-mannopyranoside

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Technology Process of phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4-tri-O-methyl-1-thio-α-D-mannopyranoside

There total 2 articles about phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4-tri-O-methyl-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: phenyl 2,3,4-tri-O-methyl-1-thio-α-D-mannopyranoside

: 65236-82-0,65236-87-5,92761-43-8,106930-83-0,134677-35-3
1,2-O-(α-methoxybenzylidene)-3,4,6-tri-O-benzoyl-β-D-mannopyranose

: 1391727-78-8
phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4-tri-O-methyl-1-thio-α-D-mannopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -30 ℃;
DOI:10.1002/ejoc.201200089

Reference yield:

: phenyl 6-O-tert-butyldiphenylsilyl-2,3,4-tri-O-methyl-1-thio-α-D-mannopyranoside

: 1391727-78-8
phenyl 6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4-tri-O-methyl-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C

2: boron trifluoride diethyl etherate / dichloromethane / -30 °C

With boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.201200089