Technology Process of C26H22F3NO4
There total 13 articles about C26H22F3NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C31H32F3NO7;
With
trifluoroacetic acid;
In
dichloromethane;
at 0 - 20 ℃;
for 0.5h;
With
sodium hydrogencarbonate;
In
water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridinium hydrobromide perbromide
2: hydrogenchloride; sodium nitrite
3: TurboGrignard
4: LiN(i-C4H9)2; N,N,N,N,-tetramethylethylenediamine
5: boron tribromide
6: TurboGrignard
With
hydrogenchloride; TurboGrignard; pyridinium hydrobromide perbromide; LiN(i-C4H9)2; N,N,N,N,-tetramethylethylenediamine; boron tribromide; sodium nitrite;
DOI:10.1021/acs.jmedchem.6b01903
- Guidance literature:
-
Multi-step reaction with 8 steps
1: nitric acid; sulfuric acid
2: sodium dithionite
3: pyridinium hydrobromide perbromide
4: hydrogenchloride; sodium nitrite
5: TurboGrignard
6: LiN(i-C4H9)2; N,N,N,N,-tetramethylethylenediamine
7: boron tribromide
8: TurboGrignard
With
hydrogenchloride; TurboGrignard; sodium dithionite; pyridinium hydrobromide perbromide; LiN(i-C4H9)2; N,N,N,N,-tetramethylethylenediamine; sulfuric acid; nitric acid; boron tribromide; sodium nitrite;
DOI:10.1021/acs.jmedchem.6b01903