benzyl 3-O-(2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl)-4-O-acetyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside

Base Information

Chemical Name:benzyl 3-O-(2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl)-4-O-acetyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside
CAS No.:1312425-29-8
Molecular Formula:C₇₂H₇₈O₂₄Si
Molecular Weight:1355.48
Hs Code.:

benzyl 3-O-(2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl)-4-O-acetyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside

Synonyms:benzyl 3-O-(2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl)-4-O-acetyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside

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Chemical Property of benzyl 3-O-(2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl)-4-O-acetyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside

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Technology Process of benzyl 3-O-(2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl)-4-O-acetyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside

There total 1 articles about benzyl 3-O-(2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl)-4-O-acetyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1312425-26-5
benzyl 4-O-acetyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside

: 1312425-28-7
ethyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside-(1->6)-2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside

: 1312425-29-8
benzyl 3-O-(2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl)-4-O-acetyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside

Guidance literature:: With N-iodo-succinimide; In dichloromethane; at -20 ℃; for 0.333333h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2011.03.109

Reference yield:

: 1312425-29-8
benzyl 3-O-(2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl)-4-O-acetyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside

: C₅₆H₆₀O₂₄

Guidance literature:: benzyl 3-O-(2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl)-4-O-acetyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside; With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -5 ℃; for 0.0833333h; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; Inert atmosphere;
DOI:10.1016/j.tet.2011.03.109

Reference yield:

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 1312425-29-8
benzyl 3-O-(2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl)-4-O-acetyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside

: C₅₆H₆₀O₂₄

: 1312425-30-1
benzyl 3-O-(2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl)-4-O-acetyl-6-O-trimethylsilyl-α-D-mannopyranoside

Guidance literature:: trimethylsilyl trifluoromethanesulfonate; benzyl 3-O-(2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl)-4-O-acetyl-6-O-tert-butyldiphenylsilyl-α-D-mannopyranoside;

With trifluorormethanesulfonic acid;
DOI:10.1016/j.tet.2011.03.109