C₁₁H₁₅ClO

Base Information

• Chemical Name: C₁₁H₁₅ClO
• CAS No.: 1083427-48-8
• Molecular Formula: C₁₁H₁₅ClO
• Molecular Weight: 198.692
• Mol file: 1083427-48-8.mol

Synonyms:C₁₁H₁₅ClO

Chemical Property of C₁₁H₁₅ClO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₁H₁₅ClO

There total 2 articles about C₁₁H₁₅ClO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Chloro-1-(4-hydroxy-3-methyl-phenyl)-butan-1-one (113425-30-2) → C11H15ClO (1083427-48-8)

Guidance literature:

With 10% Pd/C; hydrogen; In ethanol; at 20 ℃;

DOI:10.1002/anie.200801852

Reference yield:

ortho-cresol (95-48-7,77504-84-8) → C11H15ClO (1083427-48-8)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane / Acidic conditions; Inert atmosphere

2: triethylsilane; trifluoroacetic acid / 20 °C

With triethylsilane; trifluoroacetic acid; In dichloromethane;

DOI:10.1002/jccs.202000103

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + C11H15ClO (1083427-48-8) → C12H15ClO2 (1083427-51-3)

Guidance literature:

formaldehyd; C₁₁H₁₅ClO; With triethylamine; magnesium chloride; In tetrahydrofuran; for 4h; Inert atmosphere; Reflux;

With water; Inert atmosphere;

DOI:10.1002/anie.200801852

upstream raw materials:

4-Chloro-1-(4-hydroxy-3-methyl-phenyl)-butan-1-one

ortho-cresol

Downstream raw materials:

C₁₂H₁₅ClO₂

C₁₂H₁₅IO₂