2-(trimethylsilyl)ethyl 4-[(N¹,N²-bis(tert-butyloxycarbonyl)guanidino)methyl]-3-iodobenzoate

Base Information

• Chemical Name: 2-(trimethylsilyl)ethyl 4-[(N¹,N²-bis(tert-butyloxycarbonyl)guanidino)methyl]-3-iodobenzoate
• CAS No.: 191987-27-6
• Molecular Formula: C₂₄H₃₈IN₃O₆Si
• Molecular Weight: 619.572

Synonyms:2-(trimethylsilyl)ethyl 4-[(N¹,N²-bis(tert-butyloxycarbonyl)guanidino)methyl]-3-iodobenzoate

Chemical Property of 2-(trimethylsilyl)ethyl 4-[(N¹,N²-bis(tert-butyloxycarbonyl)guanidino)methyl]-3-iodobenzoate

Chemical Property:

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Technology Process of 2-(trimethylsilyl)ethyl 4-[(N¹,N²-bis(tert-butyloxycarbonyl)guanidino)methyl]-3-iodobenzoate

There total 1 articles about 2-(trimethylsilyl)ethyl 4-[(N¹,N²-bis(tert-butyloxycarbonyl)guanidino)methyl]-3-iodobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

tert-butyl N-[amino(tert-butoxycarbonylamino)methylene]carbamate (332882-82-3,154476-57-0) + 4-Bromomethyl-3-iodo-benzoic acid 2-trimethylsilanyl-ethyl ester → 2-(trimethylsilyl)ethyl 4-[(N1,N2-bis(tert-butyloxycarbonyl)guanidino)methyl]-3-iodobenzoate (191987-27-6)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; Ambient temperature;

DOI:10.1021/jo9704164

upstream raw materials:

tert-butyl N-[amino(tert-butoxycarbonylamino)methylene]carbamate

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