Technology Process of 2,5-DIBROMO-M-XYLENE
There total 5 articles about 2,5-DIBROMO-M-XYLENE which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-Bromo-m-xylene;
With
(1,5-cyclooctadiene)(methoxy)iridium(I) dimer; bis(pinacol)diborane; 4,4'-di-tert-butyl-2,2'-bipyridine;
In
hexane;
at 80 ℃;
Inert atmosphere;
Schlenk technique;
With
copper(ll) bromide;
In
methanol;
for 120h;
regioselective reaction;
Reflux;
DOI:10.1002/chem.201905328
- Guidance literature:
-
4-bromo-2,6-dimethylphenylamine;
With
hydrogen bromide; sodium nitrite;
In
water;
at -10 ℃;
for 1h;
With
ferrous(II) sulfate heptahydrate; aminosulfonic acid; hydrogen bromide;
In
water;
at 80 ℃;
for 1h;
DOI:10.1021/jacs.8b00277
- Guidance literature:
-
4-bromo-3,5-dimethylaniline;
With
sulfuric acid; sodium nitrite;
In
acetic acid;
at 0 - 10 ℃;
for 1h;
With
hydrogen bromide; copper(I) bromide;
In
acetic acid;
at 70 ℃;
for 2h;
DOI:10.1021/jo049571q
