c-5-(N-phenethylcarbamoyl)-1,3,5-trimethyl-r-1,c-3-cyclohexanedicarboxylic acid

Base Information

Chemical Name:c-5-(N-phenethylcarbamoyl)-1,3,5-trimethyl-r-1,c-3-cyclohexanedicarboxylic acid
CAS No.:156571-14-1
Molecular Formula:C₂₀H₂₇NO₅
Molecular Weight:361.438
Hs Code.:

Synonyms:c-5-(N-phenethylcarbamoyl)-1,3,5-trimethyl-r-1,c-3-cyclohexanedicarboxylic acid

Suppliers and Price of c-5-(N-phenethylcarbamoyl)-1,3,5-trimethyl-r-1,c-3-cyclohexanedicarboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of c-5-(N-phenethylcarbamoyl)-1,3,5-trimethyl-r-1,c-3-cyclohexanedicarboxylic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of c-5-(N-phenethylcarbamoyl)-1,3,5-trimethyl-r-1,c-3-cyclohexanedicarboxylic acid

There total 3 articles about c-5-(N-phenethylcarbamoyl)-1,3,5-trimethyl-r-1,c-3-cyclohexanedicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 107271-36-3
1,5,7-trimethyl-2,4-dioxo-3-oxabicyclo[3.3.1]nonane-7-carboxylic acid

: 64-04-0
phenethylamine

: 156571-14-1
c-5-(N-phenethylcarbamoyl)-1,3,5-trimethyl-r-1,c-3-cyclohexanedicarboxylic acid

Guidance literature:: With dmap; triethylamine; In dichloromethane;
DOI:10.1246/bcsj.70.1895

Reference yield: 60.0%

: 156-28-5
2-phenylethylamine hydrochloride

: 118537-27-2
(1R,5S,7S)-1,5,7-Trimethyl-2,4-dioxo-3-oxa-bicyclo[3.3.1]nonane-7-carboxylic acid

: 156571-14-1
c-5-(N-phenethylcarbamoyl)-1,3,5-trimethyl-r-1,c-3-cyclohexanedicarboxylic acid

Guidance literature:: With triethylamine; In dichloromethane; at 22 ℃; for 16h;
DOI:10.1021/jo00092a006

Reference yield:

: 79410-20-1
Kemp's triacid

: 156571-14-1
c-5-(N-phenethylcarbamoyl)-1,3,5-trimethyl-r-1,c-3-cyclohexanedicarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 86.5 percent / 190 °C / 0.01 Torr

2: 82 percent / Et₃N, 4-dimethylaminopyridine / CH₂Cl₂

With dmap; triethylamine; In dichloromethane;
DOI:10.1246/bcsj.70.1895