3-methylthio-5-phenyl-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-(2H)-1,2,4-triazole

Base Information

• Chemical Name: 3-methylthio-5-phenyl-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-(2H)-1,2,4-triazole
• CAS No.: 1217460-42-8
• Molecular Formula: C₃₅H₂₉N₃O₇S
• Molecular Weight: 635.697

Synonyms:3-methylthio-5-phenyl-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-(2H)-1,2,4-triazole

Chemical Property of 3-methylthio-5-phenyl-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-(2H)-1,2,4-triazole

Chemical Property:

Purity/Quality:

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Technology Process of 3-methylthio-5-phenyl-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-(2H)-1,2,4-triazole

There total 1 articles about 3-methylthio-5-phenyl-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-(2H)-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose (6974-32-9) + 3-methylthio-5-phenyl-2H-[1,2,4]triazole (7747-19-5) → 3-methylthio-5-phenyl-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-(2H)-1,2,4-triazole (1217460-42-8)

Guidance literature:

3-methylthio-5-phenyl-2H-[1,2,4]triazole; With sodium hydride; In tetrahydrofuran; at -70 ℃;

1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose; In tetrahydrofuran; at -70 ℃; for 5h;

DOI:10.1080/15257770903368377

Reference yield: 75.0%

3-methylthio-5-phenyl-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-(2H)-1,2,4-triazole (1217460-42-8) → 3-hydrazino-5-phenyl-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-(2H)-1,2,4-triazole (1217460-43-9)

Guidance literature:

With hydrazine hydrate; In ethanol; for 2h; Reflux;

DOI:10.1080/15257770903368377

upstream raw materials:

1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

3-methylthio-5-phenyl-2H-[1,2,4]triazole

Downstream raw materials:

3-hydrazino-5-phenyl-2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-(2H)-1,2,4-triazole

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