(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-[N-Cbz-Phe-Lys(ε-Alloc)-((4-aminobenzyloxy)carbonyl)amino]octadecane-1,3,4-triol

Base Information

Chemical Name:(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-[N-Cbz-Phe-Lys(ε-Alloc)-((4-aminobenzyloxy)carbonyl)amino]octadecane-1,3,4-triol
CAS No.:1613320-97-0
Molecular Formula:C₈₅H₁₃₇N₅O₁₇
Molecular Weight:1501.05
Hs Code.:

Synonyms:(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-[N-Cbz-Phe-Lys(ε-Alloc)-((4-aminobenzyloxy)carbonyl)amino]octadecane-1,3,4-triol

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Chemical Property of (2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-[N-Cbz-Phe-Lys(ε-Alloc)-((4-aminobenzyloxy)carbonyl)amino]octadecane-1,3,4-triol

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Technology Process of (2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-[N-Cbz-Phe-Lys(ε-Alloc)-((4-aminobenzyloxy)carbonyl)amino]octadecane-1,3,4-triol

There total 1 articles about (2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-[N-Cbz-Phe-Lys(ε-Alloc)-((4-aminobenzyloxy)carbonyl)amino]octadecane-1,3,4-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1541195-53-2
(2S,3S,4R)-2-amino-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)octadecane-1,3,4-triol

: 159857-90-6
N-Cbz-Phe-Lys(ε-Alloc)-4-aminobenzyl 4-nitrophenyl carbonate

: 1613320-97-0
(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-[N-Cbz-Phe-Lys(ε-Alloc)-((4-aminobenzyloxy)carbonyl)amino]octadecane-1,3,4-triol

Guidance literature:: (2S,3S,4R)-2-amino-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)octadecane-1,3,4-triol; N-Cbz-Phe-Lys(ε-Alloc)-4-aminobenzyl 4-nitrophenyl carbonate; With triethylamine; In pyridine; methanol; chloroform; at 20 ℃; for 34h; Inert atmosphere;

With triethylamine; In pyridine; for 24h; Inert atmosphere;

Reference yield: 94.0%

: 1613320-97-0
(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-[N-Cbz-Phe-Lys(ε-Alloc)-((4-aminobenzyloxy)carbonyl)amino]octadecane-1,3,4-triol

: 76-05-1
trifluoroacetic acid

: 1613320-99-2
(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-(N-Cbz-Phe-Lys-((4-aminobenzyloxy)carbonyl)amino)octadecane-1,3,4-triol TFA salt

Guidance literature:: (2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-[N-Cbz-Phe-Lys(ε-Alloc)-((4-aminobenzyloxy)carbonyl)amino]octadecane-1,3,4-triol; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dimethylamine borane; In methanol; dichloromethane; at 20 ℃; for 1.33333h; Inert atmosphere;

trifluoroacetic acid; In methanol;