pent-1-en-4-yne-1,1,3,5-tetrayltetrabenzene

Base Information

• Chemical Name: pent-1-en-4-yne-1,1,3,5-tetrayltetrabenzene
• CAS No.: 1352958-08-7
• Molecular Formula: C₂₉H₂₂
• Molecular Weight: 370.494
• Mol file: 1352958-08-7.mol

Synonyms:pent-1-en-4-yne-1,1,3,5-tetrayltetrabenzene

Chemical Property of pent-1-en-4-yne-1,1,3,5-tetrayltetrabenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of pent-1-en-4-yne-1,1,3,5-tetrayltetrabenzene

There total 2 articles about pent-1-en-4-yne-1,1,3,5-tetrayltetrabenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1,1-Diphenylethylene (530-48-3) + 1,3-diphenyl-1-propyn-3-ol (1817-49-8) → pent-1-en-4-yne-1,1,3,5-tetrayltetrabenzene (1352958-08-7)

Guidance literature:

With copper(II) bis(trifluoromethanesulfonate); 1,2-dichloro-ethane; for 0.166667h; Reflux;

DOI:10.1021/jo3026803

Reference yield: 92.0%

1,1-diphenylethanol (599-67-7) + 1,3-diphenyl-1-propyn-3-ol (1817-49-8) → pent-1-en-4-yne-1,1,3,5-tetrayltetrabenzene (1352958-08-7)

Guidance literature:

1,1-diphenylethanol; 1,3-diphenyl-1-propyn-3-ol; With toluene-4-sulfonic acid; In acetonitrile; at 20 ℃; Inert atmosphere;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 80 ℃; Inert atmosphere;

DOI:10.1039/c6cc09108c

upstream raw materials:

1,1-Diphenylethylene

1,3-diphenyl-1-propyn-3-ol

1,1-diphenylethanol