C₄₇H₄₆N₂O₇SSi

Base Information

Chemical Name:C₄₇H₄₆N₂O₇SSi
CAS No.:1092803-43-4
Molecular Formula:C₄₇H₄₆N₂O₇SSi
Molecular Weight:811.043
Hs Code.:

C<sub>47</sub>H<sub>46</sub>N<sub>2</sub>O<sub>7</sub>SSi

Synonyms:C₄₇H₄₆N₂O₇SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₇H₄₆N₂O₇SSi

Chemical Property:

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Technology Process of C₄₇H₄₆N₂O₇SSi

There total 13 articles about C₄₇H₄₆N₂O₇SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 937-63-3
p-Tolyl chlorothionoformate

: 1092803-42-3
C₃₉H₄₀N₂O₆Si

: 1092803-43-4
C₄₇H₄₆N₂O₇SSi

Guidance literature:: With dmap; In acetonitrile; at 0 ℃; for 1h;

Reference yield:

: 956485-06-6
3-O-(2-naphthylmethyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

: 1092803-43-4
C₄₇H₄₆N₂O₇SSi

Guidance literature:: Multi-step reaction with 16 steps

1.1: water; acetic acid / 16 h / 20 °C

2.1: sodium periodate / 1,4-dioxane; water / 1.67 h

3.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice

4.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C

6.2: 16.33 h / -78 - 20 °C

7.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

7.2: 4 h / 50 °C

8.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

8.2: 0.5 h

9.1: triphenylphosphine / dichloromethane / 0.5 h / 0 °C

9.2: 2 h / -78 °C

10.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 6 h / 20 °C

11.1: tetrahydrofuran; hexanes / 0.5 h / -78 °C

12.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C

13.1: sulfuric acid / 0.25 h / 20 °C

14.1: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 2 h / Cooling with ice; Reflux

15.1: ammonia / methanol / 16 h / 20 °C

16.1: dmap / acetonitrile / 1 h / 0 °C

With dmap; sodium periodate; n-butyllithium; N,O-bis-(trimethylsilyl)-acetamide; oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; ammonia; water; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil; 14.1: Vorbrugen reaction;

Reference yield:

: 1091607-89-4
(R)-1-((3aR,5R,6R,6aR)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[3,2-d][1,3]dioxol-5-yl)ethane-1,2-diol

: 1092803-43-4
C₄₇H₄₆N₂O₇SSi

Guidance literature:: Multi-step reaction with 15 steps

1.1: sodium periodate / 1,4-dioxane; water / 1.67 h

2.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice

3.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

5.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C

5.2: 16.33 h / -78 - 20 °C

6.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

6.2: 4 h / 50 °C

7.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

7.2: 0.5 h

8.1: triphenylphosphine / dichloromethane / 0.5 h / 0 °C

8.2: 2 h / -78 °C

9.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 6 h / 20 °C

10.1: tetrahydrofuran; hexanes / 0.5 h / -78 °C

11.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C

12.1: sulfuric acid / 0.25 h / 20 °C

13.1: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 2 h / Cooling with ice; Reflux

14.1: ammonia / methanol / 16 h / 20 °C

15.1: dmap / acetonitrile / 1 h / 0 °C

With dmap; sodium periodate; n-butyllithium; N,O-bis-(trimethylsilyl)-acetamide; oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; ammonia; water; sodium hydride; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil; 13.1: Vorbrugen reaction;