(9-{4-[9-(4-iodo-phenylethynyl)-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl]-phenylethynyl}-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl)-triisopropyl-silane

Base Information

• Chemical Name: (9-{4-[9-(4-iodo-phenylethynyl)-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl]-phenylethynyl}-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl)-triisopropyl-silane
• CAS No.: 862135-52-2
• Molecular Formula: C₅₁H₄₉ISi
• Molecular Weight: 816.94
• Mol file: 862135-52-2.mol

Synonyms:(9-{4-[9-(4-iodo-phenylethynyl)-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl]-phenylethynyl}-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl)-triisopropyl-silane

Chemical Property of (9-{4-[9-(4-iodo-phenylethynyl)-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl]-phenylethynyl}-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl)-triisopropyl-silane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (9-{4-[9-(4-iodo-phenylethynyl)-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl]-phenylethynyl}-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl)-triisopropyl-silane

There total 1 articles about (9-{4-[9-(4-iodo-phenylethynyl)-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl]-phenylethynyl}-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl)-triisopropyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C55H59N3Si (862135-37-3) → (9-{4-[9-(4-iodo-phenylethynyl)-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl]-phenylethynyl}-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl)-triisopropyl-silane (862135-52-2)

Guidance literature:

With methyl iodide; at 100 ℃; for 24h;

DOI:10.1021/jo050833d

Reference yield:

(9-{4-[9-(4-iodo-phenylethynyl)-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl]-phenylethynyl}-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl)-triisopropyl-silane (862135-52-2) → C42H29I

Guidance literature:

With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1021/jo050833d

Reference yield:

C46H39N3 + (9-{4-[9-(4-iodo-phenylethynyl)-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl]-phenylethynyl}-2,3-dihydro-1H-3a,7a-etheno-inden-8-ylethynyl)-triisopropyl-silane (862135-52-2) → C97H87N3Si

Guidance literature:

With triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; at 50 ℃; for 2.5h;

DOI:10.1021/jo050833d

upstream raw materials:

C₅₅H₅₉N₃Si