C₅₁H₆₈N₈O₆

Base Information

Chemical Name:C₅₁H₆₈N₈O₆
CAS No.:1613055-52-9
Molecular Formula:C₅₁H₆₈N₈O₆
Molecular Weight:889.151
Hs Code.:

C<sub>51</sub>H<sub>68</sub>N<sub>8</sub>O<sub>6</sub>

Synonyms:C₅₁H₆₈N₈O₆

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Chemical Property of C₅₁H₆₈N₈O₆

Chemical Property:

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Technology Process of C₅₁H₆₈N₈O₆

There total 23 articles about C₅₁H₆₈N₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 13734-41-3
t-Boc-L-valine

: C₃₁H₃₄N₆*4ClH

: 1613055-52-9
C₅₁H₆₈N₈O₆

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 3h; Inert atmosphere; Sealed tube;

Reference yield:

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 1613055-52-9
C₅₁H₆₈N₈O₆

Guidance literature:: Multi-step reaction with 8 steps

1: borane-THF / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere; Sealed tube

2: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere; Sealed tube

3: ammonia / methanol; water / 0 - 20 °C / Inert atmosphere; Sealed tube

4: N-iodo-succinimide / dichloromethane / 1.5 h / 0 °C / Inert atmosphere; Sealed tube

5: sodium sulfite / water; ethanol / 17 h / Reflux; Inert atmosphere; Sealed tube

6: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide; water; ethanol / 3 h / 90 °C / Inert atmosphere; Sealed tube

7: hydrogenchloride / ethyl acetate / 8 h / 20 °C / Inert atmosphere; Sealed tube

8: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere; Sealed tube

With hydrogenchloride; N-iodo-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1-hydroxy-7-aza-benzotriazole; borane-THF; ammonia; potassium carbonate; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium sulfite; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1612236-53-9
C₁₂H₁₄O

: 1613055-52-9
C₅₁H₆₈N₈O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-iodo-succinimide / tetrahydrofuran; acetonitrile / 0.17 h / Inert atmosphere; Sealed tube

1.2: 5 h / 20 °C / Inert atmosphere; Sealed tube

2.1: boron tribromide / dichloromethane / 4.16 h / -78 - 20 °C / Inert atmosphere; Sealed tube

3.1: pyridine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere; Sealed tube

3.2: 1 h / 0 - 20 °C / Inert atmosphere; Sealed tube

4.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 35 h / 90 °C / Inert atmosphere; Sealed tube

5.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 3 h / 90 °C / Inert atmosphere; Sealed tube

6.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide; water; ethanol / 3 h / 90 °C / Inert atmosphere; Sealed tube

7.1: hydrogenchloride / ethyl acetate / 8 h / 20 °C / Inert atmosphere; Sealed tube

8.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere; Sealed tube

With pyridine; hydrogenchloride; N-iodo-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1-hydroxy-7-aza-benzotriazole; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; boron tribromide; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;