(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-(1→6)-methyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Base Information

Chemical Name:(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-(1→6)-methyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside
CAS No.:137063-47-9
Molecular Formula:C₅₅H₆₀O₁₀
Molecular Weight:881.075
Hs Code.:

Synonyms:(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-(1→6)-methyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

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Chemical Property of (2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-(1→6)-methyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

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Technology Process of (2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-(1→6)-methyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

There total 15 articles about (2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-(1→6)-methyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 211801-54-6,807361-40-6
p-methylphenyl 2,3,4-tri-O-benzyl-1-thio-β-L-fucopyranoside

: 137063-47-9
(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-(1→6)-methyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: (2',3',4'-tri-O-benzyl-β-L-fucopyranosyl)-(1→6)-methyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: p-methylphenyl 2,3,4-tri-O-benzyl-1-thio-β-L-fucopyranoside; With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; N,N-dimethyl-formamide; In dichloromethane; at -10 ℃; Molecular sieve;

methyl 2,3,4-tri-O-benzyl-D-glucopyranoside; In dichloromethane; at -10 ℃; for 4.5h; optical yield given as %de; diastereoselective reaction;
DOI:10.1002/anie.201100076

Reference yield:

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 167612-35-3
2,3,4-tri-O-benzyl-1-thio-β-L-fucopyranoside

: 137063-47-9
(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-(1→6)-methyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: (2',3',4'-tri-O-benzyl-β-L-fucopyranosyl)-(1→6)-methyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With 2,4,6-tri-tert-butylpyrimidine; trifluoroethyl phenyliodonium bis((trifluoromethyl)sulfonyl)imide; In dichloromethane; at 22 ℃; for 0.1h; Overall yield = 76 %; Overall yield = 53.1 mg; Inert atmosphere;
DOI:10.1021/ol5004059

Reference yield:

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: C₃₅H₃₆O₇

: 137063-47-9
(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-(1→6)-methyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: (2',3',4'-tri-O-benzyl-β-L-fucopyranosyl)-(1→6)-methyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With bismuth(lll) trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1.5h; Overall yield = 80 %; Inert atmosphere;
DOI:10.1002/ejoc.201600747