Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran

Base Information

• Chemical Name: Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran
• CAS No.: 87162-99-0
• Molecular Formula: C₂₉H₄₁N₃P₂
• Molecular Weight: 493.612
• Mol file: 87162-99-0.mol

Synonyms:Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran

Chemical Property of Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran

There total 5 articles about Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methyl>phosphonium-chlorid (87163-19-7) → Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran (87162-99-0)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 12h; Ambient temperature;

Reference yield:

bis(diethylamino)chlorophosphine (685-83-6) → Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran (87162-99-0)

Guidance literature:

Multi-step reaction with 4 steps

1: 83 percent / toluene / 4 h / Ambient temperature

2: 72 percent / tris(dimethylamino)phosphorane / 1) Ph-Cl, 6 h, r.t., 2) hexane, reflux

3: 83 percent / toluene

4: 83 percent / NaH / tetrahydrofuran / 12 h / Ambient temperature

With sodium hydride; Hexamethylphosphorous triamide; In tetrahydrofuran; toluene;

Reference yield:

Chlorbis(diethylamino)<(triphenylphosphoranyliden)methylen>phosphoran (87162-93-4) → Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran (87162-99-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 83 percent / toluene

2: 83 percent / NaH / tetrahydrofuran / 12 h / Ambient temperature

With sodium hydride; In tetrahydrofuran; toluene;

upstream raw materials:

Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methyl>phosphonium-chlorid

bis(diethylamino)chlorophosphine

Chlorbis(diethylamino)<(triphenylphosphoranyliden)methylen>phosphoran

Chlorbis(diethylamino)phosphonium-chlorid