Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran

Base Information

Chemical Name:Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran
CAS No.:87162-99-0
Molecular Formula:C₂₉H₄₁N₃P₂
Molecular Weight:493.612
Hs Code.:

Synonyms:Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran

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Chemical Property of Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran

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Technology Process of Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran

There total 5 articles about Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 87163-19-7
Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methyl>phosphonium-chlorid

: 87162-99-0
Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 12h; Ambient temperature;

Reference yield:

: 685-83-6
bis(diethylamino)chlorophosphine

: 87162-99-0
Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / toluene / 4 h / Ambient temperature

2: 72 percent / tris(dimethylamino)phosphorane / 1) Ph-Cl, 6 h, r.t., 2) hexane, reflux

3: 83 percent / toluene

4: 83 percent / NaH / tetrahydrofuran / 12 h / Ambient temperature

With sodium hydride; Hexamethylphosphorous triamide; In tetrahydrofuran; toluene;

Reference yield:

: 87162-93-4
Chlorbis(diethylamino)<(triphenylphosphoranyliden)methylen>phosphoran

: 87162-99-0
Bis(diethylamino)(dimethylamino)<(triphenylphosphoranyliden)methylen>phosphoran

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / toluene

2: 83 percent / NaH / tetrahydrofuran / 12 h / Ambient temperature

With sodium hydride; In tetrahydrofuran; toluene;