Pent-4-enoic acid (1R,7R)-7-hydroxy-1-pentyl-dec-9-enyl ester

Base Information

• Chemical Name: Pent-4-enoic acid (1R,7R)-7-hydroxy-1-pentyl-dec-9-enyl ester
• CAS No.: 195449-37-7
• Molecular Formula: C₂₀H₃₆O₃
• Molecular Weight: 324.504
• Mol file: 195449-37-7.mol

Synonyms:Pent-4-enoic acid (1R,7R)-7-hydroxy-1-pentyl-dec-9-enyl ester

Chemical Property of Pent-4-enoic acid (1R,7R)-7-hydroxy-1-pentyl-dec-9-enyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Pent-4-enoic acid (1R,7R)-7-hydroxy-1-pentyl-dec-9-enyl ester

There total 1 articles about Pent-4-enoic acid (1R,7R)-7-hydroxy-1-pentyl-dec-9-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Pent-4-enoic acid (R)-7-oxo-1-pentyl-heptyl ester (195449-36-6) + C34H33O4Ti(1+)*C5H5(1-) → (R,R)-TADDOL (93379-48-7) + Pent-4-enoic acid (1R,7R)-7-hydroxy-1-pentyl-dec-9-enyl ester (195449-37-7)

Guidance literature:

In diethyl ether; at -78 ℃; for 4h; Product distribution;

DOI:10.1021/ja9719945

Reference yield: 87.0%

iodomethylbenzene (620-05-3) + Pent-4-enoic acid (1R,7R)-7-hydroxy-1-pentyl-dec-9-enyl ester (195449-37-7) → Pent-4-enoic acid (1R,7R)-7-benzyloxy-1-pentyl-dec-9-enyl ester (195449-38-8)

Guidance literature:

With potassium hydride; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1021/ja9719945

upstream raw materials:

Pent-4-enoic acid (R)-7-oxo-1-pentyl-heptyl ester

Downstream raw materials:

Pent-4-enoic acid (1R,7R)-7-benzyloxy-1-pentyl-dec-9-enyl ester