4-ethyl-5-(2-hydroxy-3-iodo-5-methylphenyl)-2-(piperidin-1-yl)-1,3-dithiol-2-ylium perchlorate

Base Information

• Chemical Name: 4-ethyl-5-(2-hydroxy-3-iodo-5-methylphenyl)-2-(piperidin-1-yl)-1,3-dithiol-2-ylium perchlorate
• CAS No.: 1186304-91-5
• Molecular Formula: C₁₇H₂₁INOS₂*ClO₄
• Molecular Weight: 545.847

Synonyms:4-ethyl-5-(2-hydroxy-3-iodo-5-methylphenyl)-2-(piperidin-1-yl)-1,3-dithiol-2-ylium perchlorate

Chemical Property of 4-ethyl-5-(2-hydroxy-3-iodo-5-methylphenyl)-2-(piperidin-1-yl)-1,3-dithiol-2-ylium perchlorate

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Technology Process of 4-ethyl-5-(2-hydroxy-3-iodo-5-methylphenyl)-2-(piperidin-1-yl)-1,3-dithiol-2-ylium perchlorate

There total 1 articles about 4-ethyl-5-(2-hydroxy-3-iodo-5-methylphenyl)-2-(piperidin-1-yl)-1,3-dithiol-2-ylium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

1-(2-hydroxy-3-iodo-5-methylphenyl)-1-oxobutan-2-yl-piperidine-1-carbodithioate (1186304-80-2) → 4-ethyl-5-(2-hydroxy-3-iodo-5-methylphenyl)-2-(piperidin-1-yl)-1,3-dithiol-2-ylium perchlorate (1186304-91-5)

Guidance literature:

1-(2-hydroxy-3-iodo-5-methylphenyl)-1-oxobutan-2-yl-piperidine-1-carbodithioate; With methanesulfonic acid; phosphorus pentoxide; at 20 ℃; for 0.5h;

With perchloric acid; In water;

DOI:10.1007/s00706-008-0944-y

Reference yield: 100.0%

4-ethyl-5-(2-hydroxy-3-iodo-5-methylphenyl)-2-(piperidin-1-yl)-1,3-dithiol-2-ylium perchlorate (1186304-91-5) → 2-[5-ethyl-2-(piperidin-1-yl)-1,3-dithiol-2-ylium-4-yl]6-iodo-4-methylphenolate (1186304-99-3)

Guidance literature:

With sodium hydrogencarbonate; In water; at 20 ℃; for 2h;

DOI:10.1007/s00706-008-0944-y

upstream raw materials:

1-(2-hydroxy-3-iodo-5-methylphenyl)-1-oxobutan-2-yl-piperidine-1-carbodithioate

Downstream raw materials:

2-[5-ethyl-2-(piperidin-1-yl)-1,3-dithiol-2-ylium-4-yl]6-iodo-4-methylphenolate

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