dimethyl 1-(2-methyl-1-oxo-1-phenylpropan-2-yl)hydrazine-1,2-dicarboxylate

Base Information

Chemical Name:dimethyl 1-(2-methyl-1-oxo-1-phenylpropan-2-yl)hydrazine-1,2-dicarboxylate
CAS No.:72990-97-7
Molecular Formula:C₁₄H₁₈N₂O₅
Molecular Weight:294.307
Hs Code.:

Synonyms:dimethyl 1-(2-methyl-1-oxo-1-phenylpropan-2-yl)hydrazine-1,2-dicarboxylate

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Chemical Property of dimethyl 1-(2-methyl-1-oxo-1-phenylpropan-2-yl)hydrazine-1,2-dicarboxylate

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Technology Process of dimethyl 1-(2-methyl-1-oxo-1-phenylpropan-2-yl)hydrazine-1,2-dicarboxylate

There total 4 articles about dimethyl 1-(2-methyl-1-oxo-1-phenylpropan-2-yl)hydrazine-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2446-84-6
dimethyl azodicarboxylate

: 611-70-1
phenyl isopropyl ketone

: 72990-97-7
dimethyl 1-(2-methyl-1-oxo-1-phenylpropan-2-yl)hydrazine-1,2-dicarboxylate

Guidance literature:: With 1,2,2,6,6-pentamethylpiperidine; tris(pentafluorophenyl)borate; In toluene; at 22 ℃; for 12h; Inert atmosphere;
DOI:10.1021/jacs.6b11908

Reference yield: 86.0%

: 13880-58-5
β,β-dimethyl-α-dimethylaminostyrene

: 2446-84-6
dimethyl azodicarboxylate

: 72990-97-7
dimethyl 1-(2-methyl-1-oxo-1-phenylpropan-2-yl)hydrazine-1,2-dicarboxylate

Guidance literature:: In diethyl ether; overnight;

Reference yield:

: 611-70-1
phenyl isopropyl ketone

: 72990-97-7
dimethyl 1-(2-methyl-1-oxo-1-phenylpropan-2-yl)hydrazine-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: TiCl₄ / hexane / 4 h / 0 - 5 °C

2: 86 percent / diethyl ether / overnight

With titanium tetrachloride; In diethyl ether; hexane;