di-l-menthyl bicyclo<2.2.1>heptane-2,2-dicarboxylate

Base Information

Chemical Name:di-l-menthyl bicyclo<2.2.1>heptane-2,2-dicarboxylate
CAS No.:120641-24-9
Molecular Formula:C₂₉H₄₈O₄
Molecular Weight:460.698
Hs Code.:

Synonyms:di-l-menthyl bicyclo<2.2.1>heptane-2,2-dicarboxylate

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Chemical Property of di-l-menthyl bicyclo<2.2.1>heptane-2,2-dicarboxylate

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Technology Process of di-l-menthyl bicyclo<2.2.1>heptane-2,2-dicarboxylate

There total 8 articles about di-l-menthyl bicyclo<2.2.1>heptane-2,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 120615-60-3,120708-05-6
di-l-menthyl bicyclo<2.2.1>hept-5-ene-2,2-dicarboxylate

: 120641-24-9
di-l-menthyl bicyclo<2.2.1>heptane-2,2-dicarboxylate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; diethyl ether; for 1h; under 760 Torr; Ambient temperature;

Reference yield:

: 133188-13-3,133269-72-4,133269-73-5,133319-58-1
C₃₀H₄₆O₅S₂

: 120641-24-9
Di-l-menthyl <1S,4R>-bicyclo<2.2.1>heptane-2,2-dicarboxylate

Guidance literature:: With hydrogen; nickel; In methanol; for 5h; under 760 Torr; Ambient temperature;
DOI:10.1248/cpb.38.3242

Reference yield:

: 15356-60-2
(1S,2R,5S)-(+)-menthol

: 120641-24-9
di-l-menthyl bicyclo<2.2.1>heptane-2,2-dicarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / DCC / diethyl ether / 2 h / Ambient temperature

2: 37 percent / Cu(OAc)2 / acetic acid / 3.5 h / 100 °C

3: TiCl₄ / toluene / 2 h / -78 °C

4: 94 percent / H₂ / 5percent Pd-C / methanol; diethyl ether / 1 h / 760 Torr / Ambient temperature

With copper diacetate; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; titanium tetrachloride; In methanol; diethyl ether; acetic acid; toluene;