N-[2-[(2-Bromo-6-cyano-4-nitrophenyl)azo]-5-(dipropylamino)phenyl]acetamide

Base Information

Chemical Name:N-[2-[(2-Bromo-6-cyano-4-nitrophenyl)azo]-5-(dipropylamino)phenyl]acetamide
CAS No.:83249-47-2
Molecular Formula:C21H23 Br N6 O3
Molecular Weight:487.356
Hs Code.:
European Community (EC) Number:280-317-0
DSSTox Substance ID:DTXSID00868708
Nikkaji Number:J326.765B
Mol file:83249-47-2.mol

Synonyms:83249-47-2;EINECS 280-317-0;N-[2-[(2-BROMO-6-CYANO-4-NITROPHENYL)AZO]-5-(DIPROPYLAMINO)PHENYL]ACETAMIDE;N-(2-((2-Bromo-6-cyano-4-nitrophenyl)azo)-5-(dipropylamino)phenyl)acetamide;C21H23BrN6O3;DTXSID00868708;C21-H23-Br-N6-O3;Acetamide, N-[2-[(2-bromo-6-cyano-4- nitrophenyl)azo]-5-(dipropylamino)phenyl]-;Acetamide, N-[2-[(2-bromo-6-cyano-4-nitrophenyl)azo]-5-(dipropylamino)phenyl]-;N-{2-[(2-Bromo-6-cyano-4-nitrophenyl)diazenyl]-5-(dipropylamino)phenyl}acetamide

Suppliers and Price of N-[2-[(2-Bromo-6-cyano-4-nitrophenyl)azo]-5-(dipropylamino)phenyl]acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of N-[2-[(2-Bromo-6-cyano-4-nitrophenyl)azo]-5-(dipropylamino)phenyl]acetamide

Chemical Property:

Vapor Pressure:3.74E-19mmHg at 25°C
Boiling Point:694.8°Cat760mmHg
Flash Point:374°C
PSA：130.16000
Density:1.4g/cm³
LogP:7.40188
XLogP3:5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:8
Exact Mass:486.10150
Heavy Atom Count:31
Complexity:684

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCN(CCC)C1=CC(=C(C=C1)N=NC2=C(C=C(C=C2Br)[N+](=O)[O-])C#N)NC(=O)C

Technology Process of N-[2-[(2-Bromo-6-cyano-4-nitrophenyl)azo]-5-(dipropylamino)phenyl]acetamide

There total 4 articles about N-[2-[(2-Bromo-6-cyano-4-nitrophenyl)azo]-5-(dipropylamino)phenyl]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17420-30-3
5-nitroanthranilonitrile

: 83249-47-2
N-[2-(2-Bromo-6-cyano-4-nitro-phenylazo)-5-dipropylamino-phenyl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: Br₂ / acetic acid / 4 h / Heating

2: 1) NaNO₂, conc. H₂SO₄; 2) amidosulfuric acid, HCl / 1) 2 h, r.t.; 2) water, 6 h

With hydrogenchloride; sulfuric acid; aminosulfonic acid; bromine; sodium nitrite; In acetic acid;

Reference yield:

: 621-35-2,59736-00-4
N-(3-aminophenyl)-acetamide hydrochloride

: 83249-47-2
N-[2-(2-Bromo-6-cyano-4-nitro-phenylazo)-5-dipropylamino-phenyl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / Na₂CO₃ / acetonitrile / 48 h / Heating

2: 1) NaNO₂, conc. H₂SO₄; 2) amidosulfuric acid, HCl / 1) 2 h, r.t.; 2) water, 6 h

With hydrogenchloride; sulfuric acid; aminosulfonic acid; sodium carbonate; sodium nitrite; In acetonitrile;

Reference yield:

: 108-45-2,64554-26-3,76583-20-5
m-phenylenediamine

: 83249-47-2
N-[2-(2-Bromo-6-cyano-4-nitro-phenylazo)-5-dipropylamino-phenyl]-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: HCl / H₂O / 8 h / pH = 1,5-3,5

2: 73 percent / Na₂CO₃ / acetonitrile / 48 h / Heating

3: 1) NaNO₂, conc. H₂SO₄; 2) amidosulfuric acid, HCl / 1) 2 h, r.t.; 2) water, 6 h

With hydrogenchloride; sulfuric acid; aminosulfonic acid; sodium carbonate; sodium nitrite; In water; acetonitrile;