C₆₆H₁₁₄N₄O₂S₂Si₂

Base Information

Chemical Name:C₆₆H₁₁₄N₄O₂S₂Si₂
CAS No.:1333248-82-0
Molecular Formula:C₆₆H₁₁₄N₄O₂S₂Si₂
Molecular Weight:1115.96
Hs Code.:

C<sub>66</sub>H<sub>114</sub>N<sub>4</sub>O<sub>2</sub>S<sub>2</sub>Si<sub>2</sub>

Synonyms:C₆₆H₁₁₄N₄O₂S₂Si₂

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Chemical Property of C₆₆H₁₁₄N₄O₂S₂Si₂

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Technology Process of C₆₆H₁₁₄N₄O₂S₂Si₂

There total 6 articles about C₆₆H₁₁₄N₄O₂S₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 1333248-81-9
C₄₂H₇₀Br₂N₂O₂

: 1005196-16-6
C₁₅H₃₁NSSiSn

: 1333248-82-0
C₆₆H₁₁₄N₄O₂S₂Si₂

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; for 10h; Inert atmosphere; Reflux;

Reference yield:

: 500530-83-6
1,4-bis(methoxymethyl)-2,5-didodecylbenzene

: 1333248-82-0
C₆₆H₁₁₄N₄O₂S₂Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid; hydrogen bromide / 1 h / 20 °C

2.1: iron; bromine; iodine / dichloromethane / 48 h / 40 °C

3.1: sodium hydrogencarbonate / dimethyl sulfoxide; chloroform / 12 h / 100 °C

4.1: sodium dihydrogenphosphate; sodium chlorite / water; dimethyl sulfoxide; chloroform / 12 h / 20 °C

5.1: N,N-dimethyl-formamide; thionyl chloride / 1 h / Reflux

5.2: 2 h / 0 - 20 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 10 h / Inert atmosphere; Reflux

With sodium chlorite; sodium dihydrogenphosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; hydrogen bromide; bromine; iodine; iron; sodium hydrogencarbonate; acetic acid; N,N-dimethyl-formamide; In dichloromethane; chloroform; water; dimethyl sulfoxide; toluene;

Reference yield:

: 500530-84-7
1,4-bis(bromomethyl)-2,5-didodecylbenzene

: 1333248-82-0
C₆₆H₁₁₄N₄O₂S₂Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: iron; bromine; iodine / dichloromethane / 48 h / 40 °C

2.1: sodium hydrogencarbonate / dimethyl sulfoxide; chloroform / 12 h / 100 °C

3.1: sodium dihydrogenphosphate; sodium chlorite / water; dimethyl sulfoxide; chloroform / 12 h / 20 °C

4.1: N,N-dimethyl-formamide; thionyl chloride / 1 h / Reflux

4.2: 2 h / 0 - 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 10 h / Inert atmosphere; Reflux

With sodium chlorite; sodium dihydrogenphosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; bromine; iodine; iron; sodium hydrogencarbonate; N,N-dimethyl-formamide; In dichloromethane; chloroform; water; dimethyl sulfoxide; toluene;