(1S)-(-)-5-benzyloxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid chloride

Base Information

• Chemical Name: (1S)-(-)-5-benzyloxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid chloride
• CAS No.: 905307-19-9
• Molecular Formula: C₁₈H₁₇ClO₂
• Molecular Weight: 300.785

Synonyms:(1S)-(-)-5-benzyloxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid chloride

Chemical Property of (1S)-(-)-5-benzyloxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid chloride

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Technology Process of (1S)-(-)-5-benzyloxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid chloride

There total 1 articles about (1S)-(-)-5-benzyloxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1S)-(-)-5-benzyloxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid (851431-45-3) → (1S)-(-)-5-benzyloxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid chloride (905307-19-9)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; In toluene; at 45 ℃; for 1h; Product distribution / selectivity;

Reference yield:

(6-isopropylpyridin-3-yl)[(1-vinyl-1H-pyrazol-4-yl)methyl]amine (905307-10-0) + (1S)-(-)-5-benzyloxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid chloride (905307-19-9) → (1S)-5-benzyloxy-N-(6-isopropylpyridin-3-yl)-N-[(1-vinyl-1H-pyrazol-4-yl)methyl]-1,2,3,4-tetrahydronaphthalene-1-carboxamide (905307-12-2)

Guidance literature:

With pyridine; In 1,2-dichloro-ethane; at 0 - 20 ℃; for 5h;

Reference yield:

tert-butyl 4-{[(6-isopropylpyridin-3-yl)amino]methyl}-1H-pyrazole-1-carboxylate (905307-11-1) + (1S)-(-)-5-benzyloxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid chloride (905307-19-9) → tert-butyl 4-{[{[(1S)-5-benzyloxy-1,2,3,4-tetrahydronaphthalen-1-yl]carbonyl}(6-isopropylpyridin-3-yl)amino]methyl}-1H-pyrazole-1-carboxylate (905307-14-4)

Guidance literature:

With pyridine; dmap; In dichloromethane; at 0 - 20 ℃;

upstream raw materials:

(1S)-(-)-5-benzyloxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid

Downstream raw materials:

(1S)-5-benzyloxy-N-[(1-ethyl-1H-pyrazol-4-yl)methyl]-N-(6-isopropylpyridin-3-yl)-1,2,3,4-tetrahydronaphthalene-1-carboxamide

(1S)-5-benzyloxy-N-(6-isopropylpyridin-3-yl)-N-[(1-vinyl-1H-pyrazol-4-yl)methyl]-1,2,3,4-tetrahydronaphthalene-1-carboxamide

tert-butyl 4-{[{[(1S)-5-benzyloxy-1,2,3,4-tetrahydronaphthalen-1-yl]carbonyl}(6-isopropylpyridin-3-yl)amino]methyl}-1H-pyrazole-1-carboxylate

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