(E)-(9H-fluoren-9-yl)methyl(6-hydroxy-2,2-diphenylhex-4-en-1-yl)carbamate

Base Information

Chemical Name:(E)-(9H-fluoren-9-yl)methyl(6-hydroxy-2,2-diphenylhex-4-en-1-yl)carbamate
CAS No.:1372806-81-9
Molecular Formula:C₃₃H₃₁NO₃
Molecular Weight:489.614
Hs Code.:

Synonyms:(E)-(9H-fluoren-9-yl)methyl(6-hydroxy-2,2-diphenylhex-4-en-1-yl)carbamate

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Chemical Property of (E)-(9H-fluoren-9-yl)methyl(6-hydroxy-2,2-diphenylhex-4-en-1-yl)carbamate

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Technology Process of (E)-(9H-fluoren-9-yl)methyl(6-hydroxy-2,2-diphenylhex-4-en-1-yl)carbamate

There total 4 articles about (E)-(9H-fluoren-9-yl)methyl(6-hydroxy-2,2-diphenylhex-4-en-1-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1372806-79-5
C₃₈H₃₉NO₄

: 1372806-81-9
(E)-(9H-fluoren-9-yl)methyl(6-hydroxy-2,2-diphenylhex-4-en-1-yl)carbamate

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 0 - 25 ℃; for 1.5h;
DOI:10.1002/anie.201107877

Reference yield:

: 1372806-78-4
C₂₃H₂₉NO₂

: 1372806-81-9
(E)-(9H-fluoren-9-yl)methyl(6-hydroxy-2,2-diphenylhex-4-en-1-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 3 h / 0 °C

2: toluene-4-sulfonic acid / methanol / 1.5 h / 0 - 25 °C

With toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1002/anie.201107877

Reference yield:

: 86-29-3
Diphenylacetonitrile

: 1372806-81-9
(E)-(9H-fluoren-9-yl)methyl(6-hydroxy-2,2-diphenylhex-4-en-1-yl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C

1.2: -78 - 25 °C

2.1: lithium aluminium tetrahydride / diethyl ether / 3 h / 0 - 25 °C

3.1: triethylamine / tetrahydrofuran / 3 h / 0 °C

4.1: toluene-4-sulfonic acid / methanol / 1.5 h / 0 - 25 °C

With lithium aluminium tetrahydride; sodium hydride; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1002/anie.201107877