cis-bis[diphenyl(tetrahydrofurfuryl)phosphine-O,P]rhodium(I)-hexafluorophosphate

Base Information

Chemical Name:cis-bis[diphenyl(tetrahydrofurfuryl)phosphine-O,P]rhodium(I)-hexafluorophosphate
CAS No.:106948-59-8
Molecular Formula:C₃₄H₃₈O₂P₂Rh*F₆P
Molecular Weight:788.492
Hs Code.:

Synonyms:cis-bis[diphenyl(tetrahydrofurfuryl)phosphine-O,P]rhodium(I)-hexafluorophosphate

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Chemical Property of cis-bis[diphenyl(tetrahydrofurfuryl)phosphine-O,P]rhodium(I)-hexafluorophosphate

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Technology Process of cis-bis[diphenyl(tetrahydrofurfuryl)phosphine-O,P]rhodium(I)-hexafluorophosphate

There total 1 articles about cis-bis[diphenyl(tetrahydrofurfuryl)phosphine-O,P]rhodium(I)-hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 106948-57-6
(η4-1,5-cyclooctadiene)-cis-bis[diphenyl(tetrahydrofurfuryl)phosphine]rhodium(I)-hexafluorophosphate

: 106948-59-8
cis-bis[diphenyl(tetrahydrofurfuryl)phosphine-O,P]rhodium(I)-hexafluorophosphate

Guidance literature:: In dichloromethane; under inert atmosphere, dissolving; pptg. after 15 min with ether at -40°C, filtration, washing (ether), drying in vac., elem. anal.;

Reference yield:

: 106948-59-8
cis-bis[diphenyl(tetrahydrofurfuryl)phosphine-O,P]rhodium(I)-hexafluorophosphate

: 378784-00-0,7440-16-6
rhodium

Guidance literature:: In not given; decompn. at -40°C in soln. within several hours;

Reference yield:

: 106948-59-8
cis-bis[diphenyl(tetrahydrofurfuryl)phosphine-O,P]rhodium(I)-hexafluorophosphate

: 106948-65-6
tricarbonyl-trans-bis[diphenyl(tetrahydrofurfuryl)phosphine]rhodium(I)-hexafluorophosphate

Guidance literature:: With CO; In tetrahydrofuran; bubbling of CO through a soln. of Rh-complex at -40°C until it becomes colourless; (31)P-NMR;