cis-N-(4,4-diphenyl-3-butenyl)-4-hydroxy-3-piperidinecarboxylic acid hydrochloride

Base Information

Chemical Name:cis-N-(4,4-diphenyl-3-butenyl)-4-hydroxy-3-piperidinecarboxylic acid hydrochloride
CAS No.:85375-53-7
Molecular Formula:C₂₂H₂₅NO₃*ClH
Molecular Weight:387.906
Hs Code.:

Synonyms:cis-N-(4,4-diphenyl-3-butenyl)-4-hydroxy-3-piperidinecarboxylic acid hydrochloride

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Chemical Property of cis-N-(4,4-diphenyl-3-butenyl)-4-hydroxy-3-piperidinecarboxylic acid hydrochloride

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Technology Process of cis-N-(4,4-diphenyl-3-butenyl)-4-hydroxy-3-piperidinecarboxylic acid hydrochloride

There total 2 articles about cis-N-(4,4-diphenyl-3-butenyl)-4-hydroxy-3-piperidinecarboxylic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 85375-52-6
methyl N-(4,4-diphenyl-3-butenyl)-cis-4-hydroxy-3-piperidinecarboxylate

: 85375-53-7
cis-N-(4,4-diphenyl-3-butenyl)-4-hydroxy-3-piperidinecarboxylic acid hydrochloride

Guidance literature:: With hydrogenchloride; for 2h; Heating;
DOI:10.1021/jm50001a020

Reference yield:

: 6078-95-1
4,4-diphenyl-3-butenyl bromide

: 85375-53-7
cis-N-(4,4-diphenyl-3-butenyl)-4-hydroxy-3-piperidinecarboxylic acid hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / K₂CO₃, KI / dimethylformamide / 18 h / Heating

2: 70 percent / 6 N aq. HCl / 2 h / Heating

With hydrogenchloride; potassium carbonate; potassium iodide; In N,N-dimethyl-formamide;
DOI:10.1021/jm50001a020