N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine benzylamide

Base Information

Chemical Name:N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine benzylamide
CAS No.:96896-85-4
Molecular Formula:C₂₀H₂₃N₃O₄
Molecular Weight:369.42
Hs Code.:

Synonyms:N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine benzylamide

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Chemical Property of N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine benzylamide

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Technology Process of N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine benzylamide

There total 4 articles about N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 96866-19-2
N-<3(RS)--1-oxo-2-benzylpropyl>glycine benzylamide

: 96896-85-4
N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine benzylamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 3h; Ambient temperature;
DOI:10.1021/jm00147a007

Reference yield:

: 5669-19-2
2-Benzyl-2-propenoic acid

: 96896-85-4
N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine benzylamide

Guidance literature:: Multi-step reaction with 4 steps

1: 57 percent / ethanol / 168 h / Heating

2: 98 percent / acetic anhydride / 3 h / 0 °C

3: 82 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

4: 92 percent / H₂ / 10percent Pd on charcoal / methanol / 3 h / Ambient temperature

With hydrogen; acetic anhydride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; chloroform;
DOI:10.1021/jm00147a007

Reference yield:

: 96866-14-7
2-(R,S)-benzyl-3-benzyloxyamino-propionic acid

: 96896-85-4
N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine benzylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / acetic anhydride / 3 h / 0 °C

2: 82 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

3: 92 percent / H₂ / 10percent Pd on charcoal / methanol / 3 h / Ambient temperature

With hydrogen; acetic anhydride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; chloroform;
DOI:10.1021/jm00147a007