2,2,2-trichloroethyl 2-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:2,2,2-trichloroethyl 2-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3,4-di-O-benzyl-α-L-rhamnopyranoside
CAS No.:115945-93-2
Molecular Formula:C₅₁H₅₅Cl₃O₁₁
Molecular Weight:950.35
Hs Code.:

Synonyms:2,2,2-trichloroethyl 2-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3,4-di-O-benzyl-α-L-rhamnopyranoside

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Chemical Property of 2,2,2-trichloroethyl 2-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3,4-di-O-benzyl-α-L-rhamnopyranoside

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Technology Process of 2,2,2-trichloroethyl 2-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3,4-di-O-benzyl-α-L-rhamnopyranoside

There total 3 articles about 2,2,2-trichloroethyl 2-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3,4-di-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.8%

: 61236-94-0
4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl chloride

: 115945-92-1
2,2,2-trichloroethyl 3,4-di-O-benzyl-α-L-rhamnopyranoside

: 115945-93-2
2,2,2-trichloroethyl 2-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3,4-di-O-benzyl-α-L-rhamnopyranoside

: 115945-95-4
2,2,2-trichloroethyl 2-O-(4-O-acetyl-2,3,6-tri-O-benzyl-β-D-glucopyranosyl)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; silver perchlorate; In diethyl ether; benzene; for 1h;
DOI:10.1016/S0008-6215(00)90854-1

Reference yield:

: 72599-87-2
2-O-acetyl-3,4-di-O-benzyl-6-deoxy-α-L-mannopyranosyl chloride

: 115945-93-2
2,2,2-trichloroethyl 2-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / silver triflate/1,1,3,3-tetramethylurea / CH₂Cl₂ / 18 h / Ambient temperature

2: 76.6 percent / M sodium methoxide / methanol / 4 h / Ambient temperature

3: 28.4 percent / sym-collidine/silver perchlorate / benzene; diethyl ether / 1 h

With 2,4,6-trimethyl-pyridine; sodium methylate; silver trifluoromethanesulfonate; silver perchlorate; tetramethylurea; In methanol; diethyl ether; dichloromethane; benzene;
DOI:10.1016/S0008-6215(00)90854-1

Reference yield:

: 115945-91-0
2,2,2-trichloroethyl 2-O-acetyl-3,4-di-O-benzyl-α-L-rhamnopyranoside

: 115945-93-2
2,2,2-trichloroethyl 2-O-(4-O-acetyl-2,3,6-tri-O-benzyl-α-D-glucopyranosyl)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 76.6 percent / M sodium methoxide / methanol / 4 h / Ambient temperature

2: 28.4 percent / sym-collidine/silver perchlorate / benzene; diethyl ether / 1 h

With 2,4,6-trimethyl-pyridine; sodium methylate; silver perchlorate; In methanol; diethyl ether; benzene;
DOI:10.1016/S0008-6215(00)90854-1