benzyl 3-[(diphenylmethylidene)amino]-6-ethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]pyridine-2-carboxylate

Base Information

Chemical Name:benzyl 3-[(diphenylmethylidene)amino]-6-ethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]pyridine-2-carboxylate
CAS No.:1268476-95-4
Molecular Formula:C₃₉H₃₃N₃O₄
Molecular Weight:607.709
Hs Code.:

Synonyms:benzyl 3-[(diphenylmethylidene)amino]-6-ethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]pyridine-2-carboxylate

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Chemical Property of benzyl 3-[(diphenylmethylidene)amino]-6-ethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]pyridine-2-carboxylate

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Technology Process of benzyl 3-[(diphenylmethylidene)amino]-6-ethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]pyridine-2-carboxylate

There total 7 articles about benzyl 3-[(diphenylmethylidene)amino]-6-ethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]pyridine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1013-88-3
Benzophenone imine

: 1268476-94-3
benzyl 6-ethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-3-{[(trifluoromethyl)sulfonyl]oxy}-4,5-dihydro-1H-pyrrolo[3,2-c]pyridine-2-carboxylate

: 1268476-95-4
benzyl 3-[(diphenylmethylidene)amino]-6-ethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]pyridine-2-carboxylate

Guidance literature:: With caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In toluene; at 100 ℃; for 18h; Inert atmosphere;

Reference yield:

: 30414-53-0
methyl propanoyl acetate

: 1268476-95-4
benzyl 3-[(diphenylmethylidene)amino]-6-ethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]pyridine-2-carboxylate

Guidance literature:: Multi-step reaction with 7 steps

1.1: ammonium acetate / methanol / 72 h / 10 - 35 °C

2.1: sodium ethanolate / ethanol / 15 h / 150 °C

3.1: trichlorophosphate / 0.5 h / 80 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 15 h / 10 - 35 °C

5.1: triethylamine; 1,8-diazabicyclo[5.4.0]undec-7-ene / 1,2-dimethoxyethane / 24 h / Reflux

5.2: 24 h / Reflux

6.1: pyridine / 3 h / 60 °C

7.1: caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 18 h / 100 °C / Inert atmosphere

With pyridine; ammonium acetate; sodium ethanolate; potassium carbonate; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; trichlorophosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In methanol; 1,2-dimethoxyethane; ethanol; N,N-dimethyl-formamide; toluene;

Reference yield:

: 883528-73-2
3-amino-4-methyl crotonic acid methylester

: 1268476-95-4
benzyl 3-[(diphenylmethylidene)amino]-6-ethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]pyridine-2-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium ethanolate / ethanol / 15 h / 150 °C

2.1: trichlorophosphate / 0.5 h / 80 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 15 h / 10 - 35 °C

4.1: triethylamine; 1,8-diazabicyclo[5.4.0]undec-7-ene / 1,2-dimethoxyethane / 24 h / Reflux

4.2: 24 h / Reflux

5.1: pyridine / 3 h / 60 °C

6.1: caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 18 h / 100 °C / Inert atmosphere

With pyridine; sodium ethanolate; potassium carbonate; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; trichlorophosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In 1,2-dimethoxyethane; ethanol; N,N-dimethyl-formamide; toluene;